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Molecular and crystal structure of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen -2-yl)butane-1,3-dione

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Abstract

Single crystal X-ray diffraction is used to determine the crystal and molecular structure of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen-2-yl)butane-1,3-dione. Crystallographic data for C14H8F4N2O2S are as follows: a = 8.2723(6) Å, b = 9.3009(7) Å, c = 9.9895(7) Å; α = 79.224(2)°, β = 75.851(2)°, γ = 72.337(2)°. Triclinic crystal system, P-1 space group, d x = 1.622 g/cm3, V = 704.83(9) Å3, μ = 0.286 mm−1, crystal size 0.30×0.20×0.20 mm, R1 = 0.0891, wR2 = 0.1989.

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Authors and Affiliations

  1. Baku State University, Baku, Azerbaijan

    A. M. Magerramov, R. A. Alieva, V. I. Mardanova, F. M. Chyragov & A. V. Kurbanov

  2. Vladimir State Humanitarian University, Vladimir, Russia

    K. A. Potekhin

Authors
  1. A. M. Magerramov
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  2. R. A. Alieva
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  3. V. I. Mardanova
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  4. F. M. Chyragov
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  5. A. V. Kurbanov
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  6. K. A. Potekhin
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Corresponding author

Correspondence to V. I. Mardanova.

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Original Russian Text Copyright © 2012 by A. M. Magerramov, R. A. Alieva, V. I. Mardanova, F. M. Chyragov, A. V. Kurbanov, and K. A. Potekhin

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Translated from Zhurnal Strukturnoi Khimii, Vol. 53, No. 1, pp. 205–208, January–February, 2012.

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Magerramov, A.M., Alieva, R.A., Mardanova, V.I. et al. Molecular and crystal structure of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen -2-yl)butane-1,3-dione. J Struct Chem 53, 202–205 (2012). https://doi.org/10.1134/S0022476612010295

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  • DOI: https://doi.org/10.1134/S0022476612010295

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