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Crystal structure of N,N′-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropane

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Abstract

The Schiff-base compound N,N′-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropan, (2,5-MeO-ba)2pn, is synthesized and characterized by elemental analysis, FT-IR and 1H NMR spectroscopy. The crystal structure of (2,5-MeO-ba)2pn is determined by X-ray single crystal diffraction analysis. The X-ray diffraction analysis at 120 K reveals that (2,5-MeO-ba)2pn crystallizes in the orthorhombic system, Fdd2 space group with a = 29.339(9) Å, b = 29.4073(11) Å, c = 4.4524(2) Å, V = 3840.8(3) Å3, μ = 0.72 mm−1, and Z = 8.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran

    A. D. Khalaji

  2. Institute of Physics of the ASCR, Na Slovance 2, 182 21, Prague 8, Czech Republic

    K. Fejfarova & M. Dusek

Authors
  1. A. D. Khalaji
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  2. K. Fejfarova
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  3. M. Dusek
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Corresponding author

Correspondence to A. D. Khalaji.

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Original Russian Text Copyright © 2011 by A. D. Khalaji, K. Fejfarova, and M. Dusek

The text was submitted by the authors in English. Zhurnal Strukturnoi Khimii, Vol. 52, No. 6, pp. 1168–1170, November–December, 2011.

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Khalaji, A.D., Fejfarova, K. & Dusek, M. Crystal structure of N,N′-Bis-(2,5-dimethoxybenzylidene)-1,3-diaminopropane. J Struct Chem 52, 1131–1133 (2011). https://doi.org/10.1134/S0022476611060175

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  • DOI: https://doi.org/10.1134/S0022476611060175

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