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Optical Efficiency and Spectral Resolution of the Grand, Grand-1500, and STE-1 Spectrometers

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Inorganic Materials Aims and scope

Abstract

For comparing the characteristics of the Grand, Grand-1500, and STE-1 spectrometers, which are used as a part of a scintillation atomic emission complex in a combination with an electric arc setup Potok for analysis of powdered samples by the spillage-injection method, their optical efficiency, reciprocal linear dispersion, and spectral resolution are measured in the 235–344 nm region. The spectral resolution of the Grand-1500 spectrometer is 1.5–2 times better than that of the other studied spectrometers. The resolution of the Grand and STE-1 spectrometers in the fifth diffraction order is practically the same, whereas in the fourth order the resolution of the Grand is significantly better. In the 240–270 nm region, the optical efficiency of the Grand exceeds that of the STE-1 by an order of magnitude, and by a factor of 4 in the 342 nm range. The optical efficiency of the Grand-1500 near 240 nm is slightly higher than of the STE-1, whereas at 267 and 342 nm it exceeds it by a factor of 2 and 5, respectively.

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REFERENCES

  1. Dzyuba, A.A., Labusov, V.A., and Babin, S.A., Basic exposure time optimization of a solid-state radiation detector in scintillation atomic emission spectrometry, Anal. Kontrol’, 2015, vol. 19, no. 1, pp. 6–12.

    Google Scholar 

  2. Raikhbaum, Ya.D., Fizicheskie osnovy spektral’nogo analiza (Physical Basis of Spectral Analysis), Moscow: Nauka, 1980.

    Google Scholar 

  3. Tarasov, K.I. and Khokhlov, V.V., Novyi difraktsionnyi spektrograf STE-1 i ego spektroanaliticheskie vozmozhnosti (New Diffraction Spectrograph STE-1 and Its Range of Analytical Capabilities), Leningrad: Leningr. Dom Nauchno-Tekh. Propag., 1963, no. 1.

  4. Tarasov, K.I., Spektral’nye pribory (Spectral Devices), Leningrad: Mashinostroenie, 1977.

    Google Scholar 

  5. Khokhlov, V.V. Mnogoelementnyi spektral’nyi analiz v geologii (Multielement Spectral Analysis in Geology), Leningrad: Nedra, 1986.

    Google Scholar 

  6. Labusov, V.A., Garanin, V.G., and Zarubin, I.A., New spectral systems based on MAES analyzers, Zavod. Lab., Diagn. Mater., 2017, vol. 83, no. 1–2, pp. 15–20.

    Article  Google Scholar 

  7. Labusov, V.A., Put’makov, A.N., and Bekhterev, A.V., A new multichannel spectrometer for atomic-emission spectrometry at 190–450 nm wavelengths, Anal. Kontrol’, 2005, vol. 9, no. 2, pp. 135–140.

    Google Scholar 

  8. Labusov, V.A., Put’makov, A.N., Zarubin, I.A., and Garanin, V.G., New multichannel optical spectrometers based on MAES analyzers, Zavod. Lab., Diagn. Mater., 2012, vol. 78, no. 1-2, pp. 7–13.

    Google Scholar 

  9. Babin, S.A., Labusov, V.A., Selyunin, D.O., and Dzyuba, A.A., BLPP-2000 array-based high-speed multichannel analyzers of atomic emission spectra, Zavod. Lab., Diagn. Mater., 2015, vol. 81, no. 1–2, pp. 108–113.

    Google Scholar 

  10. Garanin, V.G. and Rashchenko, V.V., “Thunder ball” programmable generators for atomic-emission spectra excitation, Zavod. Lab., Diagn. Mater., 2012, vol. 78, no. 1–2, pp. 54–58.

    Google Scholar 

  11. Shabanova, E.V., Bus’ko, A.E., and Vasil’eva, I.E., Scintillation arc atomic emission analysis of powder samples using MAES with high temporal resolution, Zavod. Lab., Diagn. Mater., 2012, vol. 78, no. 1–2, pp. 24–33.

    Google Scholar 

  12. Zarubin, I.A., Labusov, V.A., and Bokk, D.N., Optimum System for Illuminating the Entrance Slit of Grand and Ékspress Multichannel Spectrometers, Zavod. Lab., Diagn. Mater., 2015, vol. 81, no. 1-2, pp. 114–116.

    Google Scholar 

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Correspondence to V. A. Labusov.

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Translated by V. Alekseev

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Dzyuba, A.A., Labusov, V.A., Vasil’eva, I.E. et al. Optical Efficiency and Spectral Resolution of the Grand, Grand-1500, and STE-1 Spectrometers. Inorg Mater 54, 1456–1460 (2018). https://doi.org/10.1134/S0020168518140091

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  • DOI: https://doi.org/10.1134/S0020168518140091

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