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Mechanochemical synthesis of fine-particle γ-LiAlO2

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Abstract

Using thermogravimetry, in situ X-ray diffraction, room-temperature X-ray diffraction, specific surface area measurements, and particle size analysis, we have studied how preliminary mechanical activation of a mixture of aluminum hydroxide and lithium carbonate in an AGO-2 planetary mill and subsequent heat treatment of the mixture influence the synthesis of fine-particle nanostructured gamma-lithium monoaluminate. We have proposed a scheme of the structural changes accompanying the synthesis of gamma-lithium monoaluminate.

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Authors and Affiliations

  1. Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch, Russian Academy of Sciences, ul. Kutateladze 18, Novosibirsk, 630128, Russia

    V. P. Isupov, Ya. E. Trukhina, N. V. Eremina, N. V. Bulina & I. A. Borodulina

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  1. V. P. Isupov
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  2. Ya. E. Trukhina
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  3. N. V. Eremina
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  4. N. V. Bulina
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  5. I. A. Borodulina
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Correspondence to V. P. Isupov.

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Original Russian Text © V.P. Isupov, Ya.E. Trukhina, N.V. Eremina, N.V. Bulina, I.A. Borodulina, 2016, published in Neorganicheskie Materialy, 2016, Vol. 52, No. 11, pp. 1262–1270.

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Isupov, V.P., Trukhina, Y.E., Eremina, N.V. et al. Mechanochemical synthesis of fine-particle γ-LiAlO2 . Inorg Mater 52, 1189–1197 (2016). https://doi.org/10.1134/S0020168516110042

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  • DOI: https://doi.org/10.1134/S0020168516110042

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