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High-temperature hydroxyapatite-titanium interaction

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Inorganic Materials Aims and scope

Abstract

Hydroxyapatite-titanium interaction has been studied in the temperature range 700 to 1200°C with a view to designing biocompatible dispersion-hardened hydroxyapatite-matrix materials for bone implants. The sequence of phase transformations in hydroxyapatite-titanium powder mixtures during heating in air has been identified using IR spectroscopy, differential thermal analysis, and X-ray diffraction. It is shown that hydroxyapatite decomposition can be inhibited via heat treatment in an atmosphere containing carbon monoxide.

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References

  1. Veresov, A.G., Putlyaev, V.I., and Tret’yakov, Yu.D., Ross. Khim. Zh., 2000, vol. 44, no. 6, pp. 32–46.

    CAS  Google Scholar 

  2. Barinov, S.M. and Komlev, V.S., Biokeramika na osnove fosfatov kal’tsiya (Calcium Phosphate Based Bioceramics), Moscow: Nauka, 2005.

    Google Scholar 

  3. Ning, C.Q. and Zhou, Y., On the Microstructure of Biocomposites Sintered from Ti, HA and Bioactive Glass, Biomaterials, 2004, vol. 25, pp. 3379–3387.

    Article  CAS  Google Scholar 

  4. Chu, C., Xue, X., Zhu, J., and Yin, Z., Mechanical and Biological Properties of Hydroxyapatite Reinforced with 40 vol. % Titanium Particles for Use As Hard Tissue Replacement, J. Mater. Sci. Mater. Med., 2004, vol. 15, pp. 665–670.

    Article  CAS  Google Scholar 

  5. Takahashi, K., Fujishiro, Y., Yin, S., and Sato, T., Preparation and Compressive Strength of α-Tricalcium Phosphate Based Cement Dispersed with Ceramic Particles, Ceram. Int., 2004, vol. 30, pp. 199–203.

    Article  CAS  Google Scholar 

  6. Gautier, S., Champion, E., and Bernache-Assollant, D., Processing, Microstructure and Toughness of Al2O3 Platelet-Reinforced Hydroxyapatite, J. Eur. Ceram. Soc., 1997, vol. 17, pp. 1361–1369.

    Article  CAS  Google Scholar 

  7. Li, J., Fartash, B., and Hermansson, L., Hydroxyapatite-Alumina Composites and Bone-Bonding, Biomaterials, 1995, vol. 6, pp. 417–422.

    Article  Google Scholar 

  8. Rao, R.R. and Kannan, T.S., Synthesis and Sintering of Hydroxyapatite-Zirconia Composites, Mater. Sci. Eng., A, 2002, vol. 20, p. 187.

    Article  Google Scholar 

  9. Silva, V.V., Lameiras, F.S., and Dominguez, R.Z., Micro-structural and Mechanical Study of Zirconia-Hydroxyapatite (ZH) Composite Ceramics for Biomedical Applications, Compos.. Sci. Technol., 2001, pp. 301–310.

  10. Smirnov, V.V., Egorov, A.A., Barinov, S.M., and Shvorneva, L.I., Calcium Phosphate Composite Bone Cements Reinforced with Fine Titanium Particles, Dokl. Akad. Nauk, 2007, vol. 413, no. 4, pp. 489–492.

    Google Scholar 

  11. Ye, H., Liu, X.Y., and Hong, H., Characterization of Sintered Titanium/Hydroxyapatite Biocomposite Using FTIR Spectroscopy, J. Mater. Sci. Mater. Med., 2008, doi: 10.1007/s10856-008-3647-3.

  12. Yang, Y., Kim, K.-H., Agrawal, C.M., and Ong, J.L., Interaction of Hydroxyapatite-Titanium at Elevated Temperature in Vacuum Environment, Biomaterials, 2004, vol. 25, pp. 2927–2932.

    Article  CAS  Google Scholar 

  13. Berezhnaya, A.Yu., Mittova, V.O., Kostyuchenko, A.V., and Mittova, I.Ya., Solid-Phase Interaction in the Hydroxyapatite/Titanium Heterostructures upon High- Temperature Annealing in Air and Argon, Neorg. Mater., 2008, vol. 44, no. 11, pp. 1348–1351 [Inorg. Mater. (Engl. Transl.), vol. 44, no. 11, pp. 1214–1217].

    Article  Google Scholar 

  14. Lidin, R.A., Molochko, V.A., and Andreeva, V.A., Khimicheskie svoistva neorganicheskikh veshchestv (Chemical Properties of Inorganic Substances), Moscow: Khimiya, 1997.

    Google Scholar 

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Authors and Affiliations

  1. Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Leninskii pr. 49, Moscow, 119991, Russia

    A. A. Egorov, V. V. Smirnov, L. I. Shvorneva, S. V. Kutsev & S. M. Barinov

Authors
  1. A. A. Egorov
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  2. V. V. Smirnov
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  3. L. I. Shvorneva
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  4. S. V. Kutsev
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  5. S. M. Barinov
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Corresponding author

Correspondence to S. M. Barinov.

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Original Russian Text © A.A. Egorov, V.V. Smirnov, L.I. Shvorneva, S.V. Kutsev, S.M. Barinov, 2010, published in Neorganicheskie Materialy, 2010, Vol. 46, No. 2, pp. 208–211.

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Egorov, A.A., Smirnov, V.V., Shvorneva, L.I. et al. High-temperature hydroxyapatite-titanium interaction. Inorg Mater 46, 168–171 (2010). https://doi.org/10.1134/S0020168510020147

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  • DOI: https://doi.org/10.1134/S0020168510020147

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