Skip to main content
SpringerLink
Log in

Determination of boron in high-aluminum semiproduct by inductively coupled plasma atomic emission spectroscopy

  • Published:
Inorganic Materials Aims and scope

Abstract

A method to determine boron in a high-aluminum semiproduct by ICP-AES is described. The detection limit is 0.012 wt %. The iron and chromium spectral noise affecting the most sensitive boron lines is studied. It is shown that the Al2O3 matrix does not influence the intensity of the analytical signal. The ways to decompose a probe by melting together are compared.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Nemodruk, A.A. and Karalova, Z.K., Analiticheskaya Khimiya Bora (Analytical Chemistry of Boron), Moscow: Nauka, 1964.

    Google Scholar 

  2. Lozinskaya, E.F. and Dedkov, Yu.M., Zavod. Lab., 2006, vol. 72, no. 8, pp. 9–12.

    CAS  Google Scholar 

  3. Uehara, N., Yamaguchi, K., and Shimizu, T., Anal. Sci., 2001, vol. 17, no. 12, p. 1421.

    Article  CAS  Google Scholar 

  4. Sah, R.N. and Brown, P.N., Plant Soil, 1997, vol. 193, nos.1-2, pp. 15–33.

    Article  CAS  Google Scholar 

  5. Pupyshev, A.A. and Danilova, D.A., Atomno-emissionnyi spektralínyi analiz s induktivno-svyazannoi plazmoi n tleyuschim razryadom po Grimu (Grimme Atomic Emsiision Spectral Analysis with Inductively Coupled Plasma), Ekaterinburg: GOU VPO UGTU-UPI, 2002.

    Google Scholar 

  6. Dolganyuk, I.M., Dobrinskaya, A.M., and Favinskii, I.Ya., Zavod. Lab., 1990, vol. 56, no. 3, pp. 96–100.

    CAS  Google Scholar 

  7. Rivera, C.M., The investigation of boron measurement utilizing Varian Vista-MPX simultaneous ICP-OES with radial viewing and CETAC technologies ultrasconic nebulizer, Varian.

  8. Sun, D.H., Waters, L.K., and Mawhinney, T.P., J. Anal. At. Spectrum., 1997, vol. 12, no. 6, pp. 675–679.

    Article  CAS  Google Scholar 

  9. Karpov, Yu.A. and Savostin, A.P., Metody probootbora i probopodtotovki (Methods of Sampling), Moscow: BINOM. Laboratoriya znanii, 2003.

    Google Scholar 

  10. Osnovy analiticheskoi khimii (Foundations of Analytical Chemistry), Zolotov, Yu.A., Ed., Moscow: Vysshaya Shkola, 2004.

    Google Scholar 

  11. Gulens, J. and Leeson, P.K., Anal. Chem., 1980, vol. 52, pp. 2235–2237.

    Article  CAS  Google Scholar 

  12. Dolaberidze, L.D., Kamkamidze, D.K., Ikhetiani, N.A., et al., Zavod. Lab., 1983, vol. 49, no. 10, pp. 4–5.

    CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Lipetsk State Technical University, Lipetsk, Russia

    I. V. Nerobeeva & T. N. Ermolaeva

Authors
  1. I. V. Nerobeeva
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. T. N. Ermolaeva
    View author publications

    You can also search for this author in PubMed Google Scholar

Additional information

Original Russian Text © I.V. Nerobeeva, T.N. Ermolaeva, 2009, published in Zavodskaya Laboratoriya. Diagnostika materialov, 2009, Vol. 45, No. 14, pp. 3–6.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Nerobeeva, I.V., Ermolaeva, T.N. Determination of boron in high-aluminum semiproduct by inductively coupled plasma atomic emission spectroscopy. Inorg Mater 45, 1580–1583 (2009). https://doi.org/10.1134/S002016850914012X

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S002016850914012X

Keywords

Search

Navigation