Abstract
The current state and specific features of analytical methods using microwave heating are analyzed. Output laboratory microwave systems are described, such as dryers; muffle furnaces for ashing, burning, and alloying at atmospheric and increased pressure; and systems for decomposition and extraction. The possibilities and trends of the application of microwave radiation for intensification of the analytical operations of sample preparation, in particular, sorption and extraction concentration, are considered. Examples of using microwave radiation for obtaining substances and materials with analytical and technological purposes are given.
Similar content being viewed by others
References
Microwave-Enhanced Chemistry. Fundamentals, Sample Preparation and Application, Kingston, H.M. and Haswell, S.J., Eds., Washington, DC: American Chemical Society, 1997.
Nüchter, M., Ondruschka, B., Bonrath, W., and Gum, A., Green Chem., 2004, vol. 6, no. 3, pp. 128–141.
Lew, A., Krutzik, P.O., Hart, M.E., and Chamberlin, A.R., J. of Combinational Chem., 2002, vol. 4, no. 2, pp. 95–105.
Kubrakova, I.V., Uspekhi khimii, 2002, vol. 71, no. 4, pp. 327–340.
Perreux, L. and Loupy, A., Tetrahedron, 2001, vol. 57, no. 45, pp. 9199–9233.
Romanova, N.N., Gravis, A.G., and Zyk, N.V., Uspekhi khimii, 2005, vol. 74, no. 11, pp. 1059–1105.
Elander, N., Jones, J.R., Lu, S.Y., and Stone-Elander, S., Chem. Soc. Rev, 2000, vol. 29, no. 4, pp. 239–249.
Mingos, D.M.P. and Baghurst, D.R., Chem. Soc. Rev., 1991, vol. 20, no. 1, pp. 1–47.
Introduction to Microwave Sample Preparation, Theory and Practice, Kingston, H.M. and Jassie, L.V., Eds., Washington, DC: American Chemical Society, 1988 (Probopodgotovka v mikrovolnovykh pechakh. Teoria I praktika, Kingston, H.M. and Jassie, L.V., Eds., Moscow: Mir, 1991.
Karre, S.O., Angew. Chem. Int., 2004, vol. 43, no. 46, pp. 6250–6284.
De la Hoz, A., Diaz-Ortiz, Á., and Moreno, A., Chem. Soc. Rev., 2005, vol. 34, no. 2, pp. 164–178.
Thiebaut, J.M., Roussy, G., Medjram, M., Seyfield, L., Garin, F., and Maire, J., Catal. Lett, 1993, vol. 21, nos. 1–2, p. 133.
Chatakondu, K., Green, M.L.H., Mingos, D.M.P., and Reynolds, S.M., J. Chem. Soc. Commun., 1989, no. 20, pp. 1515–1517.
Hayes, B.L., Microwave Synthesis. Chemistry at the Speed of Light, Matthew, NC: CEM Publishing, 2002.
Kubrakova, I.V., Zhurnal analiticheskoi khimii, 2000, vol. 55, no. 12, pp. 1239–1249.
Abu-Samra, A., Morris, J.S., and Koirtyohann, S.R., Analytical Chem., 1975, vol. 47, no. 8, pp. 1475–1477.
Xu, Y., Chen, X., and Hu, Z., Analyt. Chem. Acta, 1994, vol. 292, no. 1–2, pp 191–199.
Li, G., Xu, Y., Chen, X., and Hu, Z., Analyt. Lett., 1995, vol. 28, no. 12, pp. 2227–2238.
Xu, Y.J. and Hu, Z.D., Analyt. Lett., 1994, vol. 27, no. 4, pp. 793–805.
Chen, X.G., Xu, H.P., Dong, L.J., Liu, H.T., Zeng, Y.B., and Hu, Z.D., Analyt. and Bioanalyt. Chem., 2002, vol. 373, no. 8, pp. 883–888.
Zeng, Y.B., Xu, H.P., Liu, H.T., Wang, K.T., Chen, X.G., Hu, Z.D., and Fan, B.T., Talanta, 2001, vol. 54, no. 4, pp. 603–609.
Wang, H., Zhou, Y., Li, Q., Chen, X., and Hu, Z., Analyt. Chim. Acta, 2001, vol. 429, no. 2, pp. 207–213.
Paré, J., Bélanger, and Stafford, S, Trends Analyt. Chem., 1994, vol. 13, no. 4, pp. 176–184.
Camel, V, Trends Analyt. Chem., 2000, vol. 19, no. 4, pp. 229–248.
Smith, F.E. and Arsenault, E.A., Talanta, 1996, vol. 43, no. 8, pp. 1207–1268.
Chakraborty, R., Das, A.K., Cerrera, M.L., and de la Guardia, M., Fresenius J. Analyt. Chem., 1996, vol. 355, no. 1, pp. 99–111.
Kingston, H.M., Inductively Coupled Plasma Mass Spectrometry, Montaser, A., Ed., New York, Chichester, Weinheim, Brisbane, Singapore, and Toronto: Wiley-VCH, 1998, p. 33.
Jin, Q., Liang, F., Zhang, H., Zhao, L., Huan, Y., and Song, D., Trends Analyt. Chem., 1999, vol. 18, no. 7, pp. 479–484.
Kubrakova, I.V., Kudinova, T.F., and Kuz’min, N.M., Koordinatsionnaya khimiya, 1998, vol. 24, no. 2, pp. 131–135.
Bashilov, A.V., Fedorova, A.A., and Runov, V.K., Zhurnal organicheskoi khimii, 2000, vol. 55, no. 12, pp. 1250–1255.
Bashilov, A.V., Kuz’min, N.M., Nesterov, A.A., and Runov, V.K., Zhurnal neorganicheskoi khimii, 2000, vol. 45, no. 4, pp. 743–751.
Bashilov, A.V., Lanskaya, S.Yu., and Zolotov, Yu.A., Zhurnal organicheskoi khimii, vol. 58, no. 9, pp. 948–954.
Dedkov, Yu.M., Korsakova, N.V., and Radugina, O.G., Zhurnal analiticheskoi khimii, vol. 55, no. 12, pp. 1256–1259.
Morosanova, E.I., Velikorodnyi, A.A., Zolotov, Yu.A., and Skornyakov, V.I., Zhurnal analiticheskoi khimii, 2000, vol. 55, no. 12, pp. 1265–1269.
Toropchenova, E.S., Ezerskaya, N.A., Kubrakova, I.V., Kudinova, T.F., and Kiseleva, I.N., Koordinatsionnaya khimiya, 1999, vol. 25, no. 5, pp. 352–355.
Ezerskaya, N.A., Toropchenova, E.S., Kaprielov, V.B., Kiseleva, I.N., and Belov, S.F., Zhurnal analiticheskoi khimii, 2004, vol. 59, no. 11, pp. 1213–1217.
Ezerskaya, N.A., Toropchenova, E.S., Pachgin, D.B., and Kiseleva, I.N., Zhurnal analiticheskoi khimii, 2004, vol. 59, no.3, pp. 332–335.
Toropchenova, E.S., Ezerskaya, N.A., and Kiseleva, I.N., Zavodskaya laboratoriya. Diagnostika materialov, 2004, vol. 70, no. 9, pp. 25–28.
Ezerskaya, N.A., Toropchenova, E.S., Kubrakova, I.V., Krasheninnikova, S.V., Kudinova, T.F., Fomina, T.A., and Kiseleva, I.N., Zhurnal analiticheskoi khimii, 2000, vol. 55, no. 12, pp. 1260–1264.
Makarov, D.F., Kovaleva, O.V., and Gordienko, V.A., Zavodskaya laboratoriya. Diagnostika materialov, 2003, vol. 69, no. 12, pp. 21–23.
Sur, U.K., Marken, F., Rees, N., Compton, R.G., and Seager, R., J. of Electroanalyt. Chem., 2004, vol. 573, no. 1, pp. 175–182.
Sur, U.K., Marken, F., Coles, B.A., Compton, R.G., and Dupont, J., Chem. Comm., 2004, vol. 24, no. 24, pp. 2816–2817.
Ghanem, M.A., Compton, R.G., Coles, B.A., Canals, A., and Marken, F., The analyst, 2005, vol. 130, no. 10, pp. 1425–1431.
Konno, H. and Sasaki, Y., Chem. Lett., 2003, vol. 32, no. 3, pp. 252–253.
Jasimuddin, S., Byabartta, P., Mostafa, G., Lu, T.-H., and Sinha, C., Polyhedron, 2004, vol. 23, no. 5, pp. 727–733.
Wu, F. and Thummel, R.P., Inorg. Chim. Acta, 2002, vol. 327, no. 1, pp. 26–30.
Mainchin, B., Kettish, P., and Knapp, G., Fresenius J. Analyt. Chem., 2000, vol. 366, no. 1, pp. 26–29.
Koshcheeva, I.Ya., Belen’kaya, S.N., and Kurbakova, I.V., Abstracts of Papers, Int. Congress on Analytical Sciences, 2006, p. 860.
Nóbrega, J.A., Trevizan, L.C., Araújo, G.C.L, and Nogueira, A.R.A., Spectrochimia Acta. Part B: Atomie Spectroscopy, 2002, vol. 57, no. 12, pp. 1855–1876.
Link, D.D. and Kingston, H.M., Analyt. Chem., 2000, vol. 72, no. 13, pp. 2908–2913.
Kubrakova, I.V., Myasoedova, G.B., Eremin, S.A., Pletnev, I.V., Mokhodoeva, O.B., Morozova, V.A., and Khachatryan, K.S., Metody I ob’ekty khimicheskogo analiza, 2006, vol. 1, no. 1, pp. 27–34.
Kubrakova, I.V., Myasoedova, G.V., Shumskaya, T.V., Kudinova, T.F., Zakharchenko, E.A., and Mokhodoeva, O.B., Zhurnal analiticheskoi khimii, 2005, vol. 60, no. 5, pp. 536–542.
Kubrakova, I.V., Kudinova, T.F., Formanovskii, A.A., Kuz’min, N.M., Tsysin, G.I., and Zolotov, Yu.A., Analyst, 1994, vol. 11, pp. 2477–2480.
Analiticheskaya khimiya metallov platinovoi gruppy: Sbornik obzornykh statei, Zolotov, Yu. A., Varshal, G.M., and Ivanov, V.M., Eds., Moscow: Editorial URSS, 2003.
Kuz’min, N.M., Dementiev, A.V., Kubrakova, I.V., and Myasoedova, G.V., Zhurnal analiticheskoi khimii, 1990, vol. 45, no. 1, pp. 46–50.
Mokhdoeva, O.B., Zakharchenko, E.A., Myasiedova, G.V., and Kurakova, I.V., Blagorodnye I redkie metally Sibiri I Dal’nego Vostoka: rudoobrazuyushchie sistemy mestoriozhdenii kompleksnykh I netraditsionnykh tipov rud. Materialy nauchnoi konferentsii, Irkutsk: Izd. Inst. Geogr. SO RAN, 2005, vol. 2, pp. 231–234.
Mokhodoeva, O.B., Myasoedova, G.V., and Kubrakova, I.V., Zhurnal analiticheskoi khimii, 2007 (in press).
Kubrakova, I.V., Myasoedova, G.V., Shumskaya, T.V., Zakharchenko, E.A., Kudinova, T.F., Mend. Comm., 2003, vol. 13, no. 6, pp. 249–250.
Luque-García, J.L. and Luque de Castro, M.D., Trends in Analyt. Chem., 2003, vol. 22, no. 2, pp. 90–98.
Morozova, V.S., Eremin, S.A., Nesterenko, P.N., Kluev, N.A., Shelepchikov, A.A., and Kubrakova, I.V., Zhurnal analiticheskoi khimii, 2007 (in press).
Pletnev, I.V., Smirnova, S.V., Khachatryan, K.S., and Zernov, V.V., Zhurnal RkhO imeni D.I.Mendeleeva, 2004, vol. 58, no. 6, pp. 51–58.
Nguyen, H.P., Matondo, H., and Baboulene, M., Green Chem., 2003, vol. 5, no. 3, pp. 303–305.
Hoffman, J., Nüchter, M., Ondrushka, B., and Wasserscheid, P., Green Chem., 2003, vol. 5, no. 3, pp. 296–299.
Camel, V., Analyst, 2001, vol. 126, no. 7, pp. 1182–1193.
Dean, J.R. and Xiong, G., Trends Analyt. Chem., 2000, vol. 19, no. 9, pp. 553–564.
Macutkiewicz, E., Rompa, M., and Zygmunt, B., Crit. Rev. Analyt. Chem., 2003, vol. 33, no. 1, pp. 1–17.
Lopez-Avila, V., Crit. Rev. Analyt. Chem., 1999, vol. 29, no. 3, pp. 195–230.
Sangkhi, R. and Kannamkumaratkh, S.S., Zhurnal analiticheskoi knimii, 2004, vol. 59, no. 11, pp. 1145–1149.
Martens, D., Gferer, M., Wenzl, T., Zhang, A., Gawlik, B.M., Schramm K.-W., Lankmayr, E., and Kettrup, A., Analyt. Bioanalyt. Chem., 2002, vol. 372, no. 4, pp. 562–568.
Cortazar, E., Bartolomé, L., Delgado, A., Etxebarria, N., Fernández, L.A., Usobiaga, A., and Zuloaga, O., Analyt. Chim. Acta, 2006, vol. 534, no. 2, pp. 177–355.
Microwaves in Organic Synthesis, Loupy, A., Ed., Weinheim: Wiley-VCH, 2002.
Siu, M., Yaylayan, V.A., Bélanger, J.M.R., and Paré, J.R.J., Tetrahedron Lett., 2005, vol. 46, no. 21, pp. 3737–3739.
Siu, M., Yaylayan, V.A., Bélanger, J.M.R., and Paré, J.R.J., Tetrahedron Lett., 2005, vol. 46, no. 33, pp. 5543–5545.
Dikusar, M.A., Kubrakova, I.V., Chinarev, A.A., and Bovin, N.V., Bioorganicheskaya knimiya, 2001, vol. 27, no. 6, pp. 457–461.
Petrova, N.V., Evtushenko, A.M., Chikhacheva, I.P., Zubov, V.P., and Kubrakova, I.V., Zhurnal prikladnoi khimii, 2005, vol. 78, no. 7, pp. 1178–1182.
Ziegler, M., Monney, V., Stoeckli-Evans, H., Von Zelewsky, A., Sasaki, I., Dupic, G., Daran, J.-C., and Balvoine, G.G.A., J. Chem. Soc., Dalton Trans., 1999, vol. 999, no. 5, pp. 667–675.
Yoshikawa, N., Masuda, Y., Matsumura-Inoue, T., Chem. Lett., 2000, vol. 29, no. 10, pp. 1206–1207.
Xiao, X., Sakamoto, J., Tanabe, M., Yamazaki, S., Yamabe, S., and Matsumura-Inoue, T., J. Electroanalyt. Chem., 2002, vol. 527, no. 1, pp. 33–40.
Yoshikawa, N. and Matsumura-Inoue, T., Analyt. Sciences, 2003, vol. 19, no. 5, pp. 761–765.
Pezet, F., Daran, J.C., Sasaki, I., Ait-Haddou, H., and Balavoine, G.G.A., Organomettalics, 2000, vol. 19, no. 20, pp. 4008–4015.
Rau, S., Schäfer, B., Grüßing, A., Schebesta, S., Lamm, K., Vieth, J., Görls, H., Walther, D., Rudolph, M., Grumm, U.W., and Bikner, E., Inorg. Chim. Acta, 2004, vol. 357, no. 15, pp. 4496–4503.
Matsumura-Inoue, T., Yamamoto, Y., Yoshikawa, N., Terashima, M., Youshida, Y., Fujii, A., and Yoshino, K., Opt. Materials, 2004, vol. 27, no. 2, pp. 187–191.
Lu, Q., Gao, F., and Komarneni, S., J. Materials Online, http://www.azom.com/oars.asp, 2005, vol. 1.
Gerbec, J.A., Magana, D., Washington, A., and Strouse, G.F., J. Am.Chem. Soc., 2005, vol. 127, no. 45, pp. 15791–15800.
Li, L., Qian, H., and Ren, J., Chem. Comm., 2005, no. 4, pp. 528–530.
Martínez, M.T., Callejas, M.A., Benito, A.M., Maser, W.K., Cochet, M., Andrés, J.M., Schreiber, J., Chauvet, O., and Fierro, J.L.G., Chem. Comm., 2002, no. 9, pp. 1000–1001.
Gao, F., Lu, Q., and Komarneni, S., Chem. Materials, 2005, vol. 17, no. 4, pp. 856–860.
Wang, W.W., Zhu, Y.J., Cheng, G.F., and Huang, Y.H., Materials Lett., 2006, vol. 60, no. 5, pp. 609–612.
Inada, M., Tsujimoto, H., Eguchi, Y, Enomoto, N., and Hojo, J., Fuel, 2005, vol. 84, no. 12–13, pp. 1482–1486.
Tyagi, B., Chudasama, C.D., and Jasra, R.V., Applied Clay Science, 2006, vol. 31, no. 1–2, pp. 16–28.
Lin, S.S., Wu, C.H., Sun, M.C., and Ho, Y.P., J. Amer. Soc. Mass Spectrometry, 2005, vol. 16, no. 4, pp. 581–588.
Author information
Authors and Affiliations
Additional information
Original Russian Text © I.V. Kubrakova, E.S. Toropchenova, 2008, published in Zavodskaya Laboratoriya. Diagnostika materialov, 2008, Vol. 44, No. 14, pp. 3–14.
Rights and permissions
About this article
Cite this article
Kubrakova, I.V., Toropchenova, E.S. Microwave heating for enhancing efficiency of analytical operations (Review). Inorg Mater 44, 1509–1519 (2008). https://doi.org/10.1134/S0020168508140069
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0020168508140069