Abstract
Hydrogenated graphene has been synthesized in one step by acetylene conversion in a helium plasma jet. A dc plasma torch with a diverging anode channel and a power up to 45 kW has been used to generate plasma. The obtained graphene materials have been studied by scanning electron microscopy, Raman spectroscopy, and elemental analysis. Hydrogen desorption from the samples synthesized has been studied by thermal analysis as a function of temperature. It has been found that during annealing in vacuum, the synthesis products change their morphology because of hydrogen release.
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Sofo, J.O., Chaudhari, A.S., and Barber, G.D., Phys. Rev. B: Condens. Matter, 2007, vol. 75, p. 153.
Elias, D.C., Nair, R.R., Mohiuddin, T.M.G., Morozov, S.V., Blake, P., Halsall, M.P., Ferrari, A.C., Boukhvalov, D.W., Katsnelson, M.I., Geim, A.K., and Novoselov, K.S., Science, 2009, vol. 323, p. 610.
Boukhvalov, D.W., Katsnelson, M.I., and Lichtenstein, A.I., Phys. Rev. B: Condens. Matter, 2008, vol. 77, p. 035427.
Savchenko, A., Science, 2009, vol. 323, p. 589.
Liu, L., Ryu, S., Tomasik, M.R., Stolyarova, E., Jung, N., Hybertsen, M.S., Steigerwald, M.L., Brus, L.E., and Flynn, G.W., Nano Lett., 2008, vol. 8, p. 1965.
Md. Alam, Bhuyan, S., Md. Uddin, N., Md. Islam, M., Alam Bipasha, F., and Shafayat Hossain. S., Int. Nano Lett., 2016, vol. 6, p. 65.
Amirov, R.Kh., Kiselev, V.I., Shavelkina, M.B., and Shatalova, T.B, in Materialy VI Vserossiiskoi konferentsii po nanomaterialam s elementami nauchnoi shkoly dlya molodezhi (Proceedings of VI All-Russia Conference on Nanomaterials, Including Elements of Science Training for Youth), Moscow: IMET RAN, 2016, p. 45.
Tatarova, E., Henriques, J., Luhrs, C.C., Dias, A., Phillips, J., Abrashev, A.V., and Ferreira, C.M., Appl. Phys. Lett., 2013, vol. 103, p. 134101.
Amirov, R., Shavelkina, M., Alihanov, N., Shkolnikov, E., Tyuftyaev, A., and Vorob’eva, N., J. Nanomater., 2015, vol. 2015, p. 724508.
Shavelkina, M.B., Amirov, R.Kh., and Shatalova, T.B., in Proceedings of the 13th International Conference “Films and Coatings’ 2017”, April 18–20, 2017, St. Petersburg, p. 264.
Shavelkina, M.B., Amirov, R.H., Katarzhis, V.A., and Kiselev, V.I., J. Phys.: Conf. Ser., 2016, vol. 748, p. 012021.
Isakaev, E.Kh., Sinkevich, O.A., Tyuftyaev, A.S., and Chinnov, V.F., High Temp., 2010, vol. 48, no. 1, p. 97.
Gupta, A., Chen, G., Tadigadapa, S., and Eklund, P.C., Nano Lett., 2006, vol. 6, p. 2667.
Scheffler, M., Haberer, D., Petaccia, L., Farjam, M., Schlegel, R., Baumann, D., Hanke, T., Gruneis, A., Knupfer, M., Hess, C., and Buchner, B., ACS Nano, 2012, vol. 6, no. 2012, p. 10590.
Ferrari, A.C., Meyer, J.C., Scardaci, V., Casiraghi, C., Lazzeri, M., Mauri, F., Piscanec, S., Jiang, D., Novoselov, K.S., Roth, S., and Geim, A.K., Phys. Rev. Lett., 2006, vol. 97, p. 187401.
Ferrari, A.C., Solid State Commun., 2007, vol. 143, p. 47.
Jaiswal, M., Lim, C.H.Y.X., Bao, Q., Toh, C.T., Loh, K.P., and Ozyilmaz, B., ACS Nano, 2011, vol. 5, no. 2011, p. 888.
Chen, J.-H., Cullen, W.G., Jang, C., Fuhrer, M.S., and Williams, E.D., Phys. Rev. Lett., 2009, vol. 102, p. 236805.
Skovoroda, A.A., Spitsyn, A.V., Yanchenkov, S.V., and Zubavichus, Ya.V., Vopr. At. Nauki Tekh., Ser. Termoyad. Sint., 2008, no. 3, p. 15.
Mattas, R.F., Smith, D.L., and Abdou, M.A., J. Nucl. Mater., 1984, vol. 122/123, p. 66.
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Original Russian Text © M.B. Shavelkina, R.Kh. Amirov, T.B. Shatalova, 2018, published in Khimiya Vysokikh Energii, 2018, Vol. 52, No. 4.
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Shavelkina, M.B., Amirov, R.K. & Shatalova, T.B. Synthesis of Hydrogenated Graphene during Acetylene Conversion in Helium Plasma Jet. High Energy Chem 52, 343–347 (2018). https://doi.org/10.1134/S0018143918040161
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DOI: https://doi.org/10.1134/S0018143918040161