Skip to main content
SpringerLink
Log in

Solid Phase Extraction of Polychlorinated Dibenzo-p-dioxins, Dibenzofurans, and Dioxin-like Polychlorinated Biphenyls from Fats

  • Chemistry
  • Published:
Doklady Chemistry Aims and scope Submit manuscript

Abstract

A new method for determination of polychlorinated dibenzo-p-dioxins, polychlorinated dibenzofurans, and dioxin-like polychlorinated biphenyls in fats based on the use of Carboxen 1000 and 1016 sorbents has been proposed. The use of Carboxen 1000 obviates the stage of chemical degradation of the fat matrix, thus providing high quality of the extract purification at shorter sample preparation times and a relatively small solvent consumption. The recovery values were slightly lower than in common methods of sample preparation but, nonetheless, conformed to the criteria of Russian and foreign standard methods. The method can be used to analyze animal fats and vegetable oils from food and animal feeds.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. U.S. Environmental Protection Agency. Method 1613 Tetra-through Octa-Chlorinated Dioxins and Furans by Isotope Dilution HRGC/HRMS, Washington (D.C.): Office of Water Engineering and Analysis Division, 1994.

  2. Soboleva, E.I., Soifer, V.S., Mir-Kadyrova, E.Ya., Brodkii, E.S., Feshin, D.B., Kluyev, N.A., Polyakov, N.S., and Petukhova, G.A., Int. J. Environ. Anal. Chem., 1997, vol. 68, no. 4, pp. 511–522.

    Article  CAS  Google Scholar 

  3. Kemmochi, Y., Tsutsumi, K., Arikawa, A., and Nakazawa, H., J. Chromatogr. A, 2002, vol. 977, no. 2, pp. 155–161.

    Article  CAS  PubMed  Google Scholar 

  4. Instructions for Supelco Multi-Layer Silica Gel Column and Dual-Layer Carbon Reversible Column. https://www.sigmaaldrich.com/content/dam/sigmaaldrich/docs/.../t704007.pdf

Download references

Author information

Authors and Affiliations

  1. Institute of Ecology and Evolution, Russian Academy of Sciences, Moscow, 119071, Russia

    A. A. Shelepchikov, K. A. Turbabina, E. S. Brodskii & E. Ya. Mir-Kadyrova

  2. All-Russian State Center for Quality and Standardization of Veterinary Drugs and Feed, Moscow, 123022, Russia

    A. A. Shelepchikov, K. A. Turbabina, V. V. Ovcharenko & A. A. Komarov

Authors
  1. A. A. Shelepchikov
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. K. A. Turbabina
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. E. S. Brodskii
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. E. Ya. Mir-Kadyrova
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. V. V. Ovcharenko
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. A. A. Komarov
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to A. A. Shelepchikov.

Additional information

Original Russian Text © A.A. Shelepchikov, K.A. Turbabina, E.S. Brodskii, E.Ya. Mir-Kadyrova, V.V. Ovcharenko, A.A. Komarov, 2018, published in Doklady Akademii Nauk, 2018, Vol. 481, No. 5.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Shelepchikov, A.A., Turbabina, K.A., Brodskii, E.S. et al. Solid Phase Extraction of Polychlorinated Dibenzo-p-dioxins, Dibenzofurans, and Dioxin-like Polychlorinated Biphenyls from Fats. Dokl Chem 481, 170–172 (2018). https://doi.org/10.1134/S0012500818080049

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0012500818080049

Search

Navigation