Abstract
Thiocarbamide hydrochloride single crystals forming a salt with the composition [(NH2)2CSH]+Cl− are studied by the X-ray diffraction method. The tetragonal crystals have the unit-cell parameters a = 7.556(1) Å and c = 18.329(3) Å, V = 1046.5 Å3, Z = 8, ρcalcd = 1.436 g/cm3, sp. gr. P41212, and R = 0.050. Each chloride anion in the crystal forms five hydrogen bonds with thee different cations.
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V. I. Andrianov, Kristallografiya 34(6), 1387 (1989) [Sov. Phys. Crystallogr. 34, 835 (1989)].
M. R. Truter, Acta Crystallogr. 22, 566 (1967).
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Translated from Kristallografiya, Vol. 50, No. 3, 2005, pp. 426–427.
Original Russian Text Copyright © 2005 by Gladi\(\overset{\lower0.5em\hbox{$\smash{\scriptscriptstyle\smile}$}}{l}\).
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Gladii, Y.P. X-ray diffraction study of thiocarbamide hydrochloride. Crystallogr. Rep. 50, 382–383 (2005). https://doi.org/10.1134/1.1927594
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DOI: https://doi.org/10.1134/1.1927594