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Influence of the Preparation Method on Amorphous-Crystalline Transition in Fe84B16 Alloy

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Abstract

The amorphous-crystalline transition in Fe84B16 alloys prepared by melt spinning and high-energy ball milling was studied. Time-resolved X-ray diffraction showed that the kinetics of transition into a crystalline state depends on the method of preparing a metastable alloy. In amorphous Fe84B16 alloy prepared by melt spinning, crystallization proceeded within a time period of below 1 s and was accompanied by the formation of eutectic α-Fe–Fe3B. At temperatures above 600°C, metastable phase Fe3B was found to transform into Fe2B and α-Fe. In the high-energy ball milling produced alloy, structural changes were accomplished in 4–8 s and the transition into a state with a perfect crystalline structure was caused by the growth of nanocrystallites formed during processing.

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Funding

The work was supported by the State-supported research program for the Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences (no. 44.1).

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Authors and Affiliations

  1. Merzhanov Institute of Structural Macrokinetics and Materials Science, Russian Academy of Sciences, 142432, Chernogolovka, Russia

    D. Yu. Kovalev, N. F. Shkodich, S. G. Vadchenko & A. S. Rogachev

  2. Institute of Solid State Physics, Russian Academy of Sciences, 142432, Chernogolovka, Russia

    A. S. Aronin

Authors
  1. D. Yu. Kovalev
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  2. N. F. Shkodich
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  3. S. G. Vadchenko
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  4. A. S. Rogachev
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  5. A. S. Aronin
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Corresponding author

Correspondence to D. Yu. Kovalev.

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The authors declare that they do not have any conflicts of interest.

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Translated by O. Golosova

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Kovalev, D.Y., Shkodich, N.F., Vadchenko, S.G. et al. Influence of the Preparation Method on Amorphous-Crystalline Transition in Fe84B16 Alloy. Tech. Phys. 64, 1808–1813 (2019). https://doi.org/10.1134/S1063784219120119

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  • DOI: https://doi.org/10.1134/S1063784219120119

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