Physics of the Solid State

, Volume 54, Issue 9, pp 1882–1890 | Cite as

Adhesive strength, superhardness, and the phase and elemental compositions of nanostructured coatings based on Ti-Hf-Si-N

  • A. D. Pogrebnjak
  • V. M. Beresnev
  • A. A. Demianenko
  • V. S. Baidak
  • F. F. Komarov
  • M. V. Kaverin
  • N. A. Makhmudov
  • D. A. Kolesnikov
Surface Physics and Thin Films


New superhard coatings based on Ti-Hf-Si-N with good physical and mechanical properties have been fabricated. A comparative analysis of the physical, mechanical, and tribomechanical characteristics of the coatings has been performed. The values of hardness, modulus of elasticity, elastic recovery, adhesive strength, friction coefficient, and wear rate of the coatings have been determined and calculated. The specific features of deformation and fracture of the coatings deposited on a steel substrate during the adhesion tests have been described. It has been shown that the parameters measured during scratching make it possible to distinguish the threshold values of the critical load, which lead to different (cohesive and adhesive) types of failure of the coatings during tribological tests. The stoichiometry for different series of samples with Ti-Hf-Si-N coatings has been determined using Rutherford backscattering, secondary ion mass spectrometry, and energy dispersive microanalysis.


Friction Coefficient Critical Load Adhesive Strength Continuous Stiffness Measurement Uncontrollable Impurity 
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  1. 1.
    A. D. Pogrebnyak, O. V. Sobol’, V. M. Beresnev, P. V. Turbin, S. N. Dub, G. V. Kirik, and A. E. Dmitrienko, Tech. Phys. Lett. 35(10), 925 (2009).ADSCrossRefGoogle Scholar
  2. 2.
    A. D. Pogrebnjak, M. M. Danilionok, V. V. Uglov, N. K. Erdybaeva, G. V. Kirik, S. N. Dub, V. S. Rusakov, A. P. Shypylenko, P. V. Zukovski, and Yu. Zh. Tuleushev, Vacuum 83(Suppl. 1), S235 (2009).CrossRefGoogle Scholar
  3. 3.
    A. D. Pogrebnyak, A. P. Shipilenko, Yu. Zh. Tuleushev, M. M. Danilenok, A. A. Drobyshevskaya, V. M. Beresnev, N. K. Erdybaeva, and V. V. Uglov, Russ. Phys. J. 52(12), 1317 (2009).CrossRefGoogle Scholar
  4. 4.
    V. V. Uglov, V. M. Anischik, S. V. Zlotskij, G. Abadias, and S. N. Dub, Surf. Coat. Technol. 202, 2394 (2008).CrossRefGoogle Scholar
  5. 5.
  6. 6.
    R. A. Andrievskii, G. V. Kalinnikov, N. Hellgren, P. Sandstrom, and D. V. Shtanskii, Phys. Solid State 42(9), 1671 (2000).ADSCrossRefGoogle Scholar
  7. 7.
    R. A. Andrievskii and A. M. Glezer, Phys.-Usp. 52(4), 315 (2009).ADSCrossRefGoogle Scholar
  8. 8.
    A. D. Pogrebnyak, A. P. Shpak, N. A. Azarenkov, and V. M. Beresnev, Phys.-Usp. 52(1), 29 (2009).ADSCrossRefGoogle Scholar
  9. 9.
    R. F. Zhang, A. S. Argon, and S. Veprek, Phys. Rev. B: Condens. Matter 79, 245426 (2009).ADSCrossRefGoogle Scholar
  10. 10.
    J. Musil, P. Baroch, and P. Zeman, in Plasma Surface Engineering Research and Its Practical Applications, Ed. by R. Wei (Research Signpost, Singapore, 2007), pp. 1–34.Google Scholar
  11. 11.
    R. F. Zhang, S. H. Sheng, and S. Veprek, Appl. Phys. Lett. 91, 031906 (2007).ADSCrossRefGoogle Scholar
  12. 12.
    A. D. Pogrebnjak, M. Yu. Tashmetov, A. V. Pshyk, O. V. Sobol, V. M. Beresnev, P. V. Turbin, G. V. Kirik, and M. V. Kaverin, Ceram. Eng. Sci. Proc. 31(7), 127 (2010).CrossRefGoogle Scholar
  13. 13.
    Smithells Metals Reference Book, Ed. by W. F. Gale and T. C. Totemeier (Butterworth-Heinemann, Oxford, 1976; Metallurgiya, Moscow, 1980).Google Scholar
  14. 14.
    A. D. Korotaev, V. D. Borisov, V. Yu. Mashkov, S. V. Ovchinnikov, Yu. P. Pinzhin, and A. N. Tyumentsev, Fiz. Mezomekh. 12, 79 (2009).Google Scholar

Copyright information

© Pleiades Publishing, Ltd. 2012

Authors and Affiliations

  • A. D. Pogrebnjak
    • 1
    • 2
  • V. M. Beresnev
    • 3
  • A. A. Demianenko
    • 1
  • V. S. Baidak
    • 1
  • F. F. Komarov
    • 4
  • M. V. Kaverin
    • 1
  • N. A. Makhmudov
    • 5
  • D. A. Kolesnikov
    • 6
  1. 1.Sumy State UniversitySumyUkraine
  2. 2.Kurdyumov Institute for Metal PhysicsNational Academy of Sciences of UkraineKyivUkraine
  3. 3.Karazin Kharkiv National UniversityKharkivUkraine
  4. 4.Belarusian State UniversityMinskBelarus
  5. 5.Samarkand Branch of the Tashkent University of Information TechnologySamarkandUzbekistan
  6. 6.Belgorod State UniversityBelgorodRussia

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