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Crystallography Reports

, Volume 63, Issue 7, pp 1120–1123 | Cite as

Synthesis and Structural Characterization of a Nickel Coordination Polymer Based on 4-(1H-Imidazol-1-yl)phenyl)methanone with Phthalic Acid

  • Shu-Wen SunEmail author
  • Gao-Feng Wang
  • Xiao Zhang
STRUCTURE OF ORGANIC COMPOUNDS

Abstract

A nickel coordination polymer with V-shaped ligands, {[(L1)2Ni(H2O)2] · 2(C8H5O4)}n, (L1 = 4-(1H-imidazol-1-yl)phenyl)methanone) has been synthesized under the solvothermal conditions. The structure has been determined by the single-crystal X-ray diffraction analysis and characterized by the infrared spectroscopy and elemental analysis. The crystal is crystallized in the monoclinic sp. gr. P21/c with the unit cell parameters a = 15.6387(3) Å, b = 8.0526(2) Å, c = 24.4791(6) Å, and β = 129.2350(10)°, Z = 2. The adjacent [Ni(H2O)2] units are linked by two bridging L1 ligands to form 1D looped chains, which are extended by the hydrogen bonds to yield a 3D framework.

Notes

ACKNOWLEDGMENTS

This work was financially supported by the Young Teacher Starting-up Research of Yuncheng University (YQ-2015007), Undergraduate Training Program for Innovation and Entrepreneurship of Yuncheng University (DC2017170), and Key Laboratory of Functional Inorganic Material Chemistry (Heilongjiang University), Ministry of Education.

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Copyright information

© Pleiades Publishing, Inc. 2018

Authors and Affiliations

  1. 1.Department of Applied Chemistry, Yuncheng UniversityYunchengChina
  2. 2.MIIT Key Laboratory of Critical Materials Technology for New Energy Conversion and Storage, School of Chemistry and Chemical Engineering, Harbin Institute of TechnologyHarbinChina

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