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Crystallography Reports

, Volume 63, Issue 4, pp 531–535 | Cite as

Evaluation of the Solution Stability When Reconstructing the Volume Particle Size Distribution from Small-Angle X-Ray Scattering Data for a Silicasol Solution

  • A. E. KryukovaEmail author
  • A. S. Kozlova
  • P. V. Konarev
  • V. V. Volkov
  • V. E. Asadchikov
Diffraction and Scattering of Ionizing Radiations

Abstract

The results of studying the stability of the solution to the problem for determining the volume nanoparticle size distribution using experimental small-angle X-ray scattering (SAXS) data for a silicasol solution are presented. The possibility of reconstructing solutions using indirect Fourier transform and nonlinear minimization methods for a two-component model of spherical polydisperse particles has been investigated. The results obtained are compared with the simulation data obtained previously for theoretical data sets.

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Copyright information

© Pleiades Publishing, Inc. 2018

Authors and Affiliations

  • A. E. Kryukova
    • 1
    • 2
    Email author
  • A. S. Kozlova
    • 1
  • P. V. Konarev
    • 1
    • 2
  • V. V. Volkov
    • 1
  • V. E. Asadchikov
    • 1
  1. 1.Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”Russian Academy of SciencesMoscowRussia
  2. 2.National Research Centre “Kurchatov Institute,”MoscowRussia

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