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Crystallography Reports

, Volume 59, Issue 7, pp 955–960 | Cite as

Synthesis, characterization, and crystal structure of bis[4-(3′-benzoyl)thiocarbamidophenyl]ether

  • F. AydinEmail author
  • D. Aykaç
  • N. Burcu Arslan
  • C. Kazak
Structure of Organic Compounds
  • 99 Downloads

Abstract

The title compound, bis[4-(3′-benzoyl)thiocarbamidophenyl]ether, was synthesized by the reaction of benzoylisothiocyanate with 4,4′-diaminodiphenylether in aprotic solvent. The structure was determinated by means of elemental analysis and FT-IR, 1H-NMR, 13C-NMR and MS spectroscopic techniques. The crystal structure was characterized by X-ray syngle crystal analysis: orthorhombic, sp. gr. Pnna, Z = 4. In crystal packing, there are intramolecular hydrogen bond N-H⋯O generating S(6) motif, and intermolecular hydrogen bond N-H⋯S forming R 2 2 (8) ring.

Keywords

Thiourea Benzoyl Title Compound Intramolecular Hydrogen Bond Crystallography Report 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Pleiades Publishing, Inc. 2014

Authors and Affiliations

  • F. Aydin
    • 1
    Email author
  • D. Aykaç
    • 1
  • N. Burcu Arslan
    • 2
  • C. Kazak
    • 3
  1. 1.Department of Chemistry, Science & Arts FacultyÇanakkale Onsekiz Mart UniversityÇanakkaleTurkey
  2. 2.Department of Computer Education and Instructional Technology, Faculty of EducationGiresun UniversityGiresunTurkey
  3. 3.Physics Department, Science & Art FacultyOndokuz Mayts UniversitySamsunTurkey

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