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Journal of Analytical Chemistry

, Volume 74, Issue 11, pp 1096–1103 | Cite as

Surfactant-Assisted Voltammetric Determination of Olanzapine at Amine Functionalized TiO2/Multi-Walled Carbon Nanotubes Nanocomposite

  • Majid ArvandEmail author
  • Akram Pourhabib
ARTICLES
  • 45 Downloads

Abstract

This paper describes the development and utilization of a new nanocomposite consisting of amine-functionalized TiO2/multi-walled carbon nanotubes and sodium dodecylsulfate for glassy carbon electrode modification. The nanocomposite was characterized by Fourier transform infrared spectroscopy, transmission electron microscopy and scanning electron microscopy. The modified electrode was used for electrochemical characterization of olanzapine (OLZ). The efficiency of modified electrode for electrocatalytic oxidation of OLZ was studied by cyclic voltammetry and square wave voltammetry in phosphate buffer solution (pH 7.0). Using square wave voltammetry, the prepared sensor showed good sensitivity and selectivity with low overpotential for the determination of OLZ in the ranges from 0.05 to 0.1 and 0.1 to 10 μM, with a detection limit of 8 nM. The proposed method was employed for the determination of OLZ in tablet and blood serum samples without any pretreatment steps.

Keywords:

nanocomposite amine-functionalized TiO2 surfactant olanzapine 

Notes

FUNDING

The authors are thankful to the post-graduate office of Guilan University for the support of this work.

CONFLICT OF INTEREST

The authors declare no conflict of interest.

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Copyright information

© Pleiades Publishing, Ltd. 2019

Authors and Affiliations

  1. 1.Electroanalytical Chemistry Laboratory, Faculty of Chemistry, University of GuilanRashtIran
  2. 2.Research House of Professor Reza, Education GuilanRashtIran

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