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Journal of Analytical Chemistry

, Volume 72, Issue 2, pp 217–225 | Cite as

Identification of traces of oil contamination of biogenic sediments by solid-phase extraction combined with thin layer chromatography

  • M. G. Kul’kovEmail author
  • D. S. Vorob’ev
Articles
  • 41 Downloads

Abstract

The possibility of identifying industry-related traces of oil contamination in biogenic sediments is investigated on an example of model oil-contaminated peat samples. It is shown that oil pollution of <1 wt % in biogenic samples cannot be identified using a conventional IR spectrometric procedure. An additional study of organic extracts, isolated in sample preparation, by solid-phase extraction and thin layer chromatography can detect specific oil aromatic hydrocarbons in contaminated samples uncharacteristic for background samples of the same type.

Keywords

oil pollution biogenic sediments thin layer chromatography luminescence indicators aromatic hydrocarbons alkylbenzenes gas chromatography–mass spectrometry 

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Copyright information

© Pleiades Publishing, Ltd. 2017

Authors and Affiliations

  1. 1.Center for Collective Use of Scientific EquipmentYugra State UniversityKhanty-MansiyskRussia
  2. 2.Institute of Biology, Ecology, Soil Science, Agriculture, and ForestryNational Research Tomsk State UniversityTomskRussia

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