Journal of Analytical Chemistry

, Volume 63, Issue 4, pp 361–370 | Cite as

Chromatographic study of expert and biological samples containing desomorphine

  • S. A. Savchuk
  • S. S. Barsegyan
  • I. B. Barsegyan
  • G. M. Kolesov


Expert and biological samples containing desomorphine and concomitant compounds were studied by gas chromatography, chromatography-mass spectrometry, and high-performance liquid chromatography. Some synthetic analogues of desomorphine were identified, and their chromatographic parameters and mass spectra were described. Techniques for the extraction and study of desomorphine and didehydrodesomorphine on a Milichrom A-02 liquid chromatograph were outlined. This information is important for experts in analytical toxicology and criminalistics.


Morphine Spectral Ratio Chromatographic Study Trimethylsilyl Derivative TFAA 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.


Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.


  1. 1.
    Perechen’ narkoticheskikh sredstv, psikhotropnykh veshchestv i ikh prekursorov, podlezhashchikh kontrolyu v Rossiiskoi Federatsii (List of Narcotics, Psychotropic Substances and Precursors Thereof, Subject to Control in the Russian Federation), Russian Federation Government Decree no. 681, 1998.Google Scholar
  2. 2.
    Savchuk, S.A., Simonov, E.A., Sorokin, V.I., Dorogokupets, O.B., and Vedenin, A.N., Zh. Anal. Khim., 2004, vol. 59, no. 10, p. 1059 [J. Anal. Chem. (Engl. Transl.), vol. 59, no. 10, p. 954].Google Scholar
  3. 3.
    Khromatograf Milikhrom A-02. Opredelenie veshchestv s primeneniem baz dannykh “VEZhKh-UF,” razrabotannykh v ZAO Institut khromatografii “EkoNova” (Chromatograph Milikhrom A-02. Determination of Substances Using HPLC-UV Databases Developed in the Institute of Chromatography EcoNova), Baram, G.I., Ed., Novosibirsk, 2004.Google Scholar
  4. 4.
    Ob analiticheskoi diagnostike narkoticheskikh sredstv, psikhotropnykh i drugikh toksicheskikh veshchestv v organizme cheloveka (Analytical Diagnostic of Narcotic, Psychotropic, and Toxic Substances in Human Body), order no. 289, Minzdrav RF, 1998.Google Scholar
  5. 5.
    Lisovskaya, S.B., Barsegyan, I.B., and Barsegyan, S.S., Trudy nauchno-prakticheskoi konferentsii “Nepreryvnoe poslediplomnoe obrazovanie—investitsii v zdravookhranenie Rossii” (Proc. of Conf. on Continuous Post-Graduate Education as an Investments in Public Health of Russia), Moscow, 2005.Google Scholar

Copyright information

© Pleiades Publishing, Ltd. 2008

Authors and Affiliations

  • S. A. Savchuk
    • 1
  • S. S. Barsegyan
    • 2
  • I. B. Barsegyan
    • 3
  • G. M. Kolesov
    • 4
  1. 1.National Research Center on AddictionsMinistry of Health and Social Development of the Russian FederationMoscowRussia
  2. 2.Russian Federal Drug Control ServiceKemerovo Regional AdministrationKemerovoRussia
  3. 3.Chemical Toxicological LaboratoryGUZ Regional Clinical Narcological DispensaryKemerovoRussia
  4. 4.Vernadsky Institute of Geochemistry and Analytical ChemistryRussian Academy of SciencesMoscowRussia

Personalised recommendations