Petroleum Chemistry

, Volume 59, Issue 8, pp 854–859 | Cite as

Influence of the Precursor Preparation Procedure on the Physicochemical Properties of Silicoaluminophosphate SAPO-11

  • I. A. Shamanaeva (Tiuliukova)Email author
  • E. V. Parkhomchuk


The effect of different approaches to the mixing of precursors (different durations of agitation with a magnetic stirrer, ultrasonic treatment of a precursor suspension) on the time required for the subsequent crystallization of SAPO-11 has been studied. Ultrasonic treatment reduces the duration of hydrothermal synthesis from 24 to 1 h and the overall time of preparation of SAPO-11 from 27 to 3 h.


SAPO-11 silicoaluminophosphate crystallization crystallization time ultrasound 



The authors are grateful to the following staff members of the Institute of Catalysis assistance in instrumental studies N.A. Alekseeva (XRD), T.Ya. Efimenko and A.A. Leonova (N2/77K), and N.A. Rudina (SEM).


This work was supported by the Ministry of Education and Science of the Russian Federation (RFMEFI60417X0159, title of the agreement: “Development of methods for hydrotreating of vacuum residue into high-quality marine fuels on macroporous catalysts”).


  1. 1.
    J. M. Campelo, F. Lafont, and J. M. Marinas, Appl. Catal., A 170, 139 (1998).Google Scholar
  2. 2.
    J. M. Campelo, F. Lafont, and J. M. Marinas, Zeolites 15, 97 (1995).CrossRefGoogle Scholar
  3. 3.
    S. Subramanian, A. Mitra, C. V. V. Satyanarayana, and D. K. Chakrabarty, Appl. Catal., A 159, 229 (1997).Google Scholar
  4. 4.
    T. Matsuda, T. Kimura, E. Herawati, et al., Appl. Catal., A 136, 19 (1996).Google Scholar
  5. 5.
    D. Fan, P. Tian, S. Xu, et al., New J. Chem. 40, 4236 (2016).CrossRefGoogle Scholar
  6. 6.
    Q. Yang, M. Li, C. Zeng, and L. Zhang, Chem.-Eur. J. 19, 365 (2013).CrossRefGoogle Scholar
  7. 7.
    Z. Chen, W. Song, S. Zhu, et al., RSC Adv. 7, 4656 (2017).CrossRefGoogle Scholar
  8. 8.
    Q. Wu, I. Nartey Oduro, Y. Huang, and Y. Fang, Microporous Mesoporous Mater. 218, 24 (2015).CrossRefGoogle Scholar
  9. 9.
    H. Yang, X. Liu, G. Lu, and Y. Wang, Microporous Mesoporous Mater. 225, 144 (2016).CrossRefGoogle Scholar
  10. 10.
    B. Li, P. Tian, Y. Qi, et al., Chin. J. Catal. 34, 593 (2013).CrossRefGoogle Scholar
  11. 11.
    C. M. López, V. Escobar, M. E. Arcos, et al., Catal. Today 133–135, 120 (2008).CrossRefGoogle Scholar
  12. 12.
    C. M. López, F. J. Machado, J. Goldwasser, et al., Zeolites 19, 133 (1997).CrossRefGoogle Scholar
  13. 13.
    H. Shao, J. Chen, X. Chen, et al., Phase Transitions 88, 396 (2015).CrossRefGoogle Scholar
  14. 14.
    N. Venkatathri, S. G. Hegde, V. Ramaswamy, and S. Sivasanker, Microporous Mesoporous Mater. 23, 277 (1998).CrossRefGoogle Scholar
  15. 15.
    B. Zhang, J. Xu, F. Fan, et al., Microporous Mesoporous Mater. 147, 212 (2012).CrossRefGoogle Scholar
  16. 16.
    Y. Jin, X. Chen, Q. Sun, et al., Chem.-Eur. J. 20, 17616 (2014).CrossRefGoogle Scholar
  17. 17.
    T. Wu, X. Feng, M. L. Carreon, and M. A. Carreon, J. Nanoparticle Res. 19, 93 (2017).CrossRefGoogle Scholar
  18. 18.
    G. Finger and J. Kornatowski, Appl. Spectrosc. 10, 615 (1990).Google Scholar
  19. 19.
    U. Myeong-Heon and M. Kang, J. Ind. Eng. Chem. 11, 540 (2005).Google Scholar
  20. 20.
    J. Grand, H. Awala, and S. Mintova, Cryst. Eng. Commun. 18, 650 (2016).CrossRefGoogle Scholar
  21. 21.
    F. Di Renzo, Catal. Today 41, 37 (1998).CrossRefGoogle Scholar
  22. 22.
    S. H. Jhung, J. H. Lee, and J. S. Chang, Microporous Mesoporous Mater. 112, 178 (2008).CrossRefGoogle Scholar
  23. 23.
    M. Charghand, M. Haghighi, and S. Aghamohammadi, Ultrason. Sonochem. 21, 1827 (2014).CrossRefGoogle Scholar
  24. 24.
    S. Askari and R. Halladj, Ultrason. Sonochem. 19, 554 (2012).CrossRefGoogle Scholar
  25. 25.
    H. Feng and G. V. Barbosa-Cánovas, Ultrasound Technologies for Food and Bioprocessing, Ed. by H. Feng, G. V. Barbosa-Cánovas, and J. Weiss (Springer, New York, 2010), p. 665.Google Scholar

Copyright information

© Pleiades Publishing, Ltd. 2019

Authors and Affiliations

  • I. A. Shamanaeva (Tiuliukova)
    • 1
    Email author
  • E. V. Parkhomchuk
    • 1
    • 2
  1. 1.Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of SciencesNovosibirskRussia
  2. 2.Novosibirsk State UniversityNovosibirskRussia

Personalised recommendations