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1,8-Bis[2-(diphenylphosphoryl)phenoxy-4-phenyldiazenyl)]-3,6-dioxaoctane (L): Synthesis and Complexing and Ion-Selective Properties. Crystal and Molecular Structures of L · 0.25H2O and [LiL]I3 · MePh

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Abstract

The synthesis, IR and electronic absorption spectra, and ion-selective properties of 1,8-bis[2-(diphenylphosphoryl)phenoxy-4-phenyldiazenyl]-3,6-dioxaoctane (L), a new phosphoryl podand, are described. The crystal structures of L · 0.25H2O and the synthesized complex [LiL]I3 · MePh were characterized by X-ray diffraction. The composition of the plasticized polymeric membrane of a lithium-selective electrode based on L was determined.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, 119991, Russia

    I. S. Ivanova, A. B. Ilyukhin, I. N. Polyakova & E. N. Pyatova

  2. Institute of Physiologically Active Substances, Russian Academy of Sciences, Chernogolovka, Moscow oblast, 142432, Russia

    Yu. I. Rogacheva & V. E. Baulin

  3. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences, Moscow, 199991, Russia

    G. S. Tsebrikova, V. E. Baulin & A. Yu. Tsivadze

Authors
  1. I. S. Ivanova
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  2. A. B. Ilyukhin
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  3. I. N. Polyakova
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  4. Yu. I. Rogacheva
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  5. E. N. Pyatova
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  6. G. S. Tsebrikova
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  7. V. E. Baulin
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  8. A. Yu. Tsivadze
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Correspondence to I. S. Ivanova.

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Russian Text © I.S. Ivanova, A.B. Ilyukhin, I.N. Polyakova, Yu.I. Rogacheva, E.N. Pyatova, G.S. Tsebrikova, V.E. Baulin, A.Yu. Tsivadze, 2019, published in Zhurnal Neorganicheskoi Khimii, 2019, Vol. 64, No. 2, pp. 181–189.

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Ivanova, I.S., Ilyukhin, A.B., Polyakova, I.N. et al. 1,8-Bis[2-(diphenylphosphoryl)phenoxy-4-phenyldiazenyl)]-3,6-dioxaoctane (L): Synthesis and Complexing and Ion-Selective Properties. Crystal and Molecular Structures of L · 0.25H2O and [LiL]I3 · MePh. Russ. J. Inorg. Chem. 64, 216–224 (2019). https://doi.org/10.1134/S0036023619020098

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