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Journal of Structural Chemistry

, Volume 60, Issue 10, pp 1681–1687 | Cite as

X-Ray Diffraction Study of Crystal and Molecular Structures of Azo Compounds of Two β-Diketones

  • F. N. BahmanovaEmail author
  • Sh. A. Tahirli
  • R. K. Askerov
  • S. R. Hajiyeva
  • F. M. Chyragov
Article

Abstract

Novel compounds 2-(2-(2-hydroxy-4-nitrophenyl) hydrazono)-1,3-diphenyl propane-1,3-dione and 2-(2-(2-hydroxy-4-nitrophenyl) hydrazono)-1-phenyl butane-1,3-dione are prepared on the base of β-diketones. Crystal and molecular structures of synthesized compounds are determined by X-ray diffraction analysis. The crystals are found to be monoclinic. The compounds are represented only by their hydrazo forms. The structural data for the two obtained compounds are compared with previously reported data.

Keywords

β-diketone synthesis of azo compounds X-ray diffraction analysis molecular packing hydrogen bonding 

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Notes

Conflict of Interests

The authors declare that they have no conflict of interests.

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Copyright information

© Pleiades Publishing, Ltd. 2019

Authors and Affiliations

  • F. N. Bahmanova
    • 1
    Email author
  • Sh. A. Tahirli
    • 2
  • R. K. Askerov
    • 1
  • S. R. Hajiyeva
    • 1
  • F. M. Chyragov
    • 1
  1. 1.Baku State UniversityBakuAzerbaijan
  2. 2.Lankaran State UniversityLankaranAzerbaijan

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