Abstract
In this work, multi-walled carbon nanotubes (MWNTs) were successfully reinforced in AA 4032 nanocrystalline matrix. The elemental powders of AA 4032 composites were mechanically alloyed in the high energy ball mill for 30 h to get nanocrystalline structure. The carbon nanotubes (CNTs) were added at the 29th hour of ball milling process. The morphological changes during milling were studied, using scanning electron microscope analysis and the distribution of the CNTs within the aluminum matrix was successfully revealed, using transmission electron microscope analysis. The results show that the CNTs are effectively distributed within the aluminum matrix without any structural damage. The variation in the melting point was studied using simultaneous thermal analyzer.
Similar content being viewed by others
References
Iijima, S., “Helical Microtubules of Graphitic Carbon,” Helical Microtubules of Graphitic Carbon 354:56–58 (1991).
Popov, V.N., “Carbon Nanotubes: Properties and Application,” Carbon Nanotubes: Properties and Application 43:61–102 (2004).
Iijima, S., and Ichihasi, T., “Single-Shell Carbon Nanotubes of 1-nm Diameter,” Single-Shell Carbon Nanotubes of 1-nm Diameter 363:603–605 (1993).
Ebessen, T.W., and Ajayan, P., “Large-Scale Synthesis of Carbon Nanotubes,” Large-Scale Synthesis of Carbon Nanotubes 358:220–222 (1992).
Yu, M.F., “Tensile Loading of Ropes of Single Wall Carbon Nanotubes and Their Mechanical Properties,” Tensile Loading of Ropes of Single Wall Carbon Nanotubes and Their Mechanical Properties 84:5552–5555 (2000).
Deng, C.F., Zhang, X.X., Wang, D.Z., Lin, Q., and Li, A., “Carbon Nanotubes/Aluminum Matrix Composites,” Carbon Nanotubes/Aluminum Matrix Composites 61:1725–1728 (2007).
Deng, C.F., Zhang, X.X., Wang, D.Z., and Ma, Y.X., “Calorimetric Study of Carbon Nanotubes and Aluminum,” Calorimetric Study of Carbon Nanotubes and Aluminum 61:3221–3223 (2007).
Deng, C.F., Zhang, X.X., Wang, D.Z., and Ma, Y.X., “Thermal Expansion Behaviors of Aluminum Composite Reinforced with Carbon Nanotubes,” Thermal Expansion Behaviors of Aluminum Composite Reinforced with Carbon Nanotubes 62:2301–2303 (2008).
Deng, C.F., Wang, D.Z., Zhang, X.X., and Ma, Y.X., “Mechanical Properties of ABOw+MWNTs/Al Hybrid Composites Made by Squeeze Cast Technique,” Mechanical Properties of ABOw+MWNTs/Al Hybrid Composites Made by Squeeze Cast Technique 61:3504–3506 (2007).
Esawi, A., and Morsi, K., “Carbon Nanotube-Reinforced Aluminium Strips,” Composites Part A 38: 646–650 (2008).
Esawi, A., and Morsi, K., “Effect of Mechanical Alloying Time and Carbon Nanotube (CNT) Content on the Evolution of Aluminum (Al)-CNT Composite Powders,” Effect of Mechanical Alloying Time and Carbon Nanotube (CNT) Content on the Evolution of Aluminum (Al)-CNT Composite Powders 42:4954–4959 (2007).
Esawi, A., Morsi, K., Sayed, A., Gawad, A.A., and Borah, P., “Fabrication and Properties of Dispersed Carbon Nanotube-Aluminum Composites,” Fabrication and Properties of Dispersed Carbon Nanotube-Aluminum Composites 508:167–173 (2009).
Yuan, D., Liu, Y., Xia, Y., and Chen, L., “Preparation and Characterization of Z-Shaped Carbon Nanotubes via Decomposing Magnesium Acetate,” Preparation and Characterization of Z-Shaped Carbon Nanotubes via Decomposing Magnesium Acetate 112:27–30 (2008).
Williamson, G.K., and Hall, W.H., “X-Ray Line Broadening from Filed Aluminium and Wolfram,” X-Ray Line Broadening from Filed Aluminium and Wolfram 1:22–31 (1953).
Woo, K.D., and Huo, H.W., “Effect of High Energy Ball Milling on Displacement Reaction and Sintering of Al–Mg/SiO2 Composite Powders,” Metals and Materials International, 12:45–50 (2006).
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Senthil Saravanan, M.S., Sivaprasad, K. & Kumaresh Babu, S.P. Dispersion and thermal analysis of carbon nanotube reinforced AA 4032 alloy produced by high energy ball milling. Exp Tech 37, 14–18 (2013). https://doi.org/10.1111/j.1747-1567.2011.00760.x
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1111/j.1747-1567.2011.00760.x