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Electrochemical Halogenation of the Single-Charged Anion of Dodecahydro-7,8-dicarba-nido-undecaborate

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Abstract

By means of electrochemical iodination and bromination of potassium dodecahydro-7,8-dicarba-nido-undecaborate, extracted are monoiodide and monobromide derivatives in the form of alkylammonium salts with preparative yields. Their structure is confirmed by the data of elemental analysis and IR and 11B NMR spectroscopy.

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Authors and Affiliations

  1. Institute of Physical Organic Chemistry, Belarussian Academy of Sciences, Minsk, 220072, Belarus

    V. L. Shirokii, D. A. Rudakov, A. V. Bazhanov, E. G. Zalesskaya, V. I. Potkin & N. A. Maier

  2. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, ul. Vavilova 28, Moscow, 117813, Russia

    S. V. Timofeev, P. V. Petrovskii & V. I. Bregadze

Authors
  1. V. L. Shirokii
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  2. D. A. Rudakov
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  3. A. V. Bazhanov
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  4. E. G. Zalesskaya
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  5. V. I. Potkin
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  6. N. A. Maier
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  7. S. V. Timofeev
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  8. P. V. Petrovskii
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  9. V. I. Bregadze
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Shirokii, V.L., Rudakov, D.A., Bazhanov, A.V. et al. Electrochemical Halogenation of the Single-Charged Anion of Dodecahydro-7,8-dicarba-nido-undecaborate. Russian Journal of Electrochemistry 40, 212–214 (2004). https://doi.org/10.1023/B:RUEL.0000016338.23698.61

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  • DOI: https://doi.org/10.1023/B:RUEL.0000016338.23698.61

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