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X-Ray Spectroscopic Method for Chemical Analysis of Periclase Powders

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Refractories and Industrial Ceramics Aims and scope

Abstract

An x-ray fluorescence spectroscopic analysis in the incoming inspection of raw materials for the production of periclase powders is developed. Optimum conditions for sample preparation are described and a metrological characterization of certified mixtures is given. The advantages of the newly-developed method, based on the use of a Spectroscan-V x-ray spectrometer, are emphasized.

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REFERENCES

  1. State Standard GOST 2642-97. Refractories and Refractory Raw Materials. Methods of Analysis [in Russian].

  2. State Standard GOST 26565-85. Unshaped Refractories. Sampling and Sample Preparation [in Russian].

  3. NDP MS-80-2002 Regulations. Magnesite. Mass Fraction Determination of Oxides of Magnesium, Calcium, Silicon, Aluminum, and Iron. X-ray Fluorescence Method [in Russian].

  4. MU MO 14-1-3-90 Methodological Instructions. Certification of Methods of Quantitative Chemical Analysis [in Russian], Ekaterinburg (1990).

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Authors and Affiliations

  1. Magnitogorsk Iron and Steel Works (MISW) Joint-Stock Co., Magnitogorsk, Russia

    L. V. Mironova, E. V. Murashko & L. V. Mikhailova

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  1. L. V. Mironova
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  2. E. V. Murashko
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  3. L. V. Mikhailova
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Mironova, L.V., Murashko, E.V. & Mikhailova, L.V. X-Ray Spectroscopic Method for Chemical Analysis of Periclase Powders. Refractories and Industrial Ceramics 45, 222–224 (2004). https://doi.org/10.1023/B:REFR.0000036735.22798.df

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  • DOI: https://doi.org/10.1023/B:REFR.0000036735.22798.df

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