Abstract
The present study provides a comparative analysis of the size dispersity of magnetic nanoparticles (MNPs) within magnetic fluids as obtained from atomic force microscopy (AFM) and transmission electron microscopy (TEM). Whereas the mean particle diameter obtained from the AFM data presented a reduction of about 34% as compared to the value obtained from the TEM data, the standard deviation obtained from the AFM data is twice the value found from the TEM data. Similarities and differences in the size dispersity parameters are discussed in terms of sample preparation and tip characteristics. A two-dimensional mode for the deposition of the MNPs on top of the mica substrate is discussed as well.
Similar content being viewed by others
References
Berkovsky B.M., V.F. Mecvedev & M.S. Krakov, 1993. Magnetic Fluids: Engineering Applications, Oxford University Press, New York.
Hutter J.L. & J. Bechhoefer, 1993. J. Rev. Sci. Instrum. 64,1868.
Kellar K.E., D.K. Fujii W.H.H. Gunther K. Briley-Sæbø, M. Spiller & S.H. Koenig, 1999. Magn. Res. Mater. Phys. Biol. Med. 8,207.
Konerack’a M. P. Kop¡ cansk’ y M. Antal’ýk M. Timko, C.N. Ramchand D. Lobo R.V. Mehta & R.V. Upadhyay, 1999. J. Magn. Magn. Mater. 201,427.
Lacava B.M., R.B. Azevedo L.P. Silva Z.G.M. Lacava K. Skeff Neto N. Buske A.F. Bakuzis & P.C. Morais, 2000. Appl. Phys. Lett. 77,1876.
Moore L.R., A.R. Rodriguez P.S. Williams K. McCloskey, B. Bolwell M. Nakamura J.J. Chalmers & M.J. Zborowski, 2001. J. Magn. Magn. Mater. 225,277.
Morais P.C., B.M. Lacava A.F. Bakuzis L.M. Lacava L.P. Silva, R.B. Azevedo Z.G.M. Lacava N. Buske W.C. Nunes & M.A. Novak, 2001. J. Magn. Magn. Mater. 226–230, 1899.
Payet B., D. Vincent L. Delaunay & G.J. Noyel, 1998. J. Magn. Magn. Mater. 186,168.
Pereira A.R., G.R. Gonc¸alves A.F. Bakuzis P.C. Morais, R.B. Azevedo & K. Skeff Neto, 2001. IEEE Trans. Magn. 37, 2657.
Rabelo D., E.C.D. Lima A.C. Reis W.C. Nunes M.A. Novak, V.K. Garg A.C. Oliveira & P.C. Morais, 2001. Nano Lett. 1, 105.
Sayle R.A., F. Milne & E.J. White, 1995. Trends Biochem. Sci. 20, 374.
Viau G., F. Fi’ evet-Vincent, F. Fi’ evet P. Toneguzzo F. Ravel & O.J. Acher, 1997. Appl. Phys. 81, 2749.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Silva, L., Lacava, Z., Buske, N. et al. Atomic force microscopy and transmission electron microscopy of biocompatible magnetic fluids: A comparative analysis. J Nanopart Res 6, 209–213 (2004). https://doi.org/10.1023/B:NANO.0000034597.83456.6e
Issue Date:
DOI: https://doi.org/10.1023/B:NANO.0000034597.83456.6e