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Titania-Doped Silica Fibers Prepared by Electrospinning and Sol-Gel Process

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Abstract

Titania-doped silica fibers were prepared by electrospinning of the sol of silica containing titania. The electrospun fibers had ribbon type morphology. The fibers had significant quantities of hydroxyl groups of Si—OH and Ti—OH. The fibers did not have crystalline structure. Diameters of the fibers were reduced by solvent evaporation and calcination. The hydroxyl groups on the fibers disappeared by calcination. The hydroxyl groups, M—OH (M≡Si, Ti) were changed to M—O—M by intermolecular and intramolecular condensation reactions.

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References

  1. J.K. Walters, J.S. Rigden, P.J. Dirken, M.E. Smith, W.S. Howells, and R.J. Newport, Chem. Phys. Lett. 264, 539 (1997).

    Article  Google Scholar 

  2. H. Yamashita, S. Kawasaki, Y. Ichihara, M. Harada, M. Takeuchi, M. Anpo, G. Stewart, M.A. Fox, C. Louis, and M. Che, J. Phys. Chem. B 102, 5870 (1998).

    Article  Google Scholar 

  3. K. Kosuge and P.S. Singh, J. Phys. Chem. B 103, 3563 (1999).

    Google Scholar 

  4. M. Hori and M. Toki, J. Sol-Gel Sci. Technol. 19, 349 (2000).

    Article  Google Scholar 

  5. M. Jung, J. Sol-Gel Sci. Technol. 19, 563 (2000).

    Article  Google Scholar 

  6. W. Que, Y. Zhou, Y.L. Lam, Y. C. Chan, Z. Sun, S.D. Chen, H.P. Li, and C.H. Kam, J. Mater. Sci. Lett. 19, 1247 (2000).

    Google Scholar 

  7. W. Que, Z. Sun, Y.L. Lam, Y.C. Chan, and C.H. Kam, J. Phys. D: Appl. Phys. 34, 471 (2001).

    Article  Google Scholar 

  8. J.E. Goncalves, S.C. Castro, A.Y. Ramos, M.C.M. Alves, and Y. Gushikem, J. Elec. Spec. 114-116, 307 (2001).

    Google Scholar 

  9. C.J. Briner, K.D. Keefer, D.W. Schaefer, R.A. Assink, B.D. Kay, and C.S. Ashley, J. Non-Crystal. Solids 63, 45 (1984).

    Google Scholar 

  10. L.L. Hench and J.K. West, Chem. Rev. 90, 33 (1990).

    Google Scholar 

  11. J. Zarzycki, J. Sol-Gel Sci. Technol. 8, 17 (1997).

    Article  Google Scholar 

  12. D.R. Uhlmann, G. Teowee, and J. Boulton, J. Sol-Gel Sci. Technol. 8, 1083 (1997).

    Google Scholar 

  13. A.K. McEvoy, C. McDonagh, and B.D. MacCraith, J. Sol-Gel Sci. Technol. 8, 1121 (1997).

    Google Scholar 

  14. T. Peltola, M. Jokinen, S. Veittola, H. Rahiala, and A. Yli-Urpo, Biomaterials 22, 589 (2001).

    Google Scholar 

  15. M. Zhang, Y. Bando, and K. Wada, J. Mater. Sci. Lett. 20, 167 (2001).

    Google Scholar 

  16. H. Nakamura and Y. Matsui, J. Am. Chem. Soc. 117, 2651 (1995).

    Google Scholar 

  17. S. Kobayashi, K. Hanabusa, N. Hamasaki, M. Kimura, and H. Shirai, Chem. Mater. 12, 1523 (2000). Titania-Doped Silica Fibers Prepared by Electrospinning and Sol-Gel Process 221

    Google Scholar 

  18. M. Zhang, Y. Bando, K. Wada, and K. Kurashima, J. Mater. Sci. Lett. 18, 1911 (1999).

    Google Scholar 

  19. R.A. Caruso, J.H. Schattka, and A. Greiner, Adv. Mater. 13, 1577 (2001).

    Google Scholar 

  20. M. Kursawe, W. Glaubitt, and A. Thierauf, J. Sol-Gel Sci. Technol. 9, 267 (1998).

    Google Scholar 

  21. Y. Xu, W. Zhou, L. Zhang, and L. Cheng, J. Mater. Proc. Technol. 101, 44 (2000).

    Google Scholar 

  22. R.L. Oréfice, L.L. Hench, A.E. Clark, and A.B. Brennan, J. Biomed. Mater. Res. 55, 460 (2001).

    Google Scholar 

  23. S. Kobayashi, K. Hanabusa, M. Suzuki, M. Kimura, and H. Shirai, Chem. Lett. 1077 (1999).

  24. J. Doshi and D.H. Reneker, J. Electrostat. 35, 151 (1995).

    Google Scholar 

  25. D.H. Reneker and I. Chun, Nanotechnology 7, 216 (1996).

    Article  Google Scholar 

  26. S. Koombhongse, W. Liu, and D.H. Reneker, J. Polym. Sci. B: Polym. Phys. 39, 2598 (2001).

    Google Scholar 

  27. S.-G. Lee, S.-S. Choi, and C.W. Joo, J. Kor. Fiber Soc. 39, 1 (2002).

    Google Scholar 

  28. M. Bognitzki, W. Czado, T. Frese, A. Schaper, M. Hellwig, M. Steinhart, A. Greiner, and J.H. Wendorff, Adv. Mater. 13, 70 (2001).

    Google Scholar 

  29. J.M. Deitzel, W. Kosik, S.H. McKnight, N.C. Beck Tan, J.M. DeSimone, and S. Crette, Polymer 43, 1025 (2002).

    Google Scholar 

  30. T. Peltola, M. Jokinen, S. Veittola, H. Rahiala, and A. Yli-Urpo, Biomaterials 22, 589 (2001).

    Google Scholar 

  31. Y. Xu, W. Zhou, L. Zhang, and L. Cheng, J. Mater. Proc. Technol. 101, 44 (2000).

    Google Scholar 

  32. H. Izutsu, F. Mizukami, T. Sashida, K. Maeda, Y. Kiyozumi, and Y. Akiyama, J. Non-Crystal. Solids 212, 40 (1997).

    Google Scholar 

  33. D.J. Kim, S.H. Hahn, S.H. Oh, and E.J. Kim, Mater. Lett. 57, 355 (2002).

    Google Scholar 

  34. W.L. Huang, S.H. Cui, K.M. Liang, Z.F. Yuan, and S.R. Gu, J. Phys. Chem. Solids 63, 645 (2002).

    Google Scholar 

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Authors and Affiliations

  1. Department of Applied Chemistry, College of Natural Sciences, Sejong University, 98 Koonja-dong, Kwangjin-gu, Seoul, 143-747, Korea

    Sung-Seen Choi

  2. Department of Textile Engineering, Chungnam National University, 220, Gung-dong, Yuseong-gu, Daejeon, 305-764, Korea

    Boyoung Chu & Seung Goo Lee

  3. Research Institute of Advanced Materials, Chungnam National University, Daejeon, 305-764, Korea

    Sung Wook Lee

  4. Department of Fiber &, Polymer Engineering, College of Engineering, Hanyang University, 17 Haengdang-dong, Seongdong-gu, Seoul, 133-791, Korea

    Sung Soon Im & Seong Hun Kim

  5. Agency for Defense Development, Yuseong-gu, Daejeon, 305-600, Korea

    Jong Kyoo Park

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  1. Sung-Seen Choi
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  2. Boyoung Chu
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  3. Seung Goo Lee
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  4. Sung Wook Lee
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  7. Jong Kyoo Park
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Choi, SS., Chu, B., Lee, S.G. et al. Titania-Doped Silica Fibers Prepared by Electrospinning and Sol-Gel Process. Journal of Sol-Gel Science and Technology 30, 215–221 (2004). https://doi.org/10.1023/B:JSST.0000039530.09380.bc

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  • DOI: https://doi.org/10.1023/B:JSST.0000039530.09380.bc

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