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Synthesis of [3H]-higenamine

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Abstract

The synthesis of [3H]-higenamine by a four steps reaction, namely condensation, cyclization, catalytic tritiation and demethoxylation is described. The acidulated product was purified by thin layer chromatography and the final component has a high specific activity and radiochemical purity.

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Authors and Affiliations

  1. China Institute of Atomic Energy, P. O. Box 275(39), Beijing, 102413, P.R. China

    Dezhu Wu & Ginfu Li

  2. Cardiovascular Institute and Fu Wai Hospital, Chinese Academy of Medical Science and Peking Union Medical College, Beijing, 100037, P.R. China

    Zheng Zhang & Baoling Chen

Authors
  1. Dezhu Wu
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  2. Zheng Zhang
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  3. Baoling Chen
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  4. Ginfu Li
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Wu, D., Zhang, Z., Chen, B. et al. Synthesis of [3H]-higenamine. Journal of Radioanalytical and Nuclear Chemistry 258, 689–691 (2003). https://doi.org/10.1023/B:JRNC.0000011772.32047.e5

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  • DOI: https://doi.org/10.1023/B:JRNC.0000011772.32047.e5

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