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Synthesis and X-ray structure analysis of 2-acetylamino-benzoic acid

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Abstract

The title compound crystallizes in the orthorhombic space group Fdd2 with unit cell parameters a = 10.848(1) Å, b = 30.264(1) Å and c = 10.577(1) Å, V = 3472.47(2) Å3, and Z = 4. The final reliability index is 0.030 for 700 observed reflections. Nitrogen of the amide group and carbon atom of the acid group deviate significantly below and above the plane of the phenyl ring. The crystal cohesion is accentuated by N—H⋅⋅⋅O and O—H⋅⋅⋅O hydrogen bonds.

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Authors and Affiliations

  1. Condensed Matter Physics Group, Post Graduate Department of Physics, University of Jammu, Jammu Tawi, 180 006, India

    Rajnikant,  Dinesh &  Kamni

  2. Department of Chemistry, Shivaji University, Kolhapur, Maharashtra, 416 004, India

    M.B. Deshmukh

Authors
  1. Rajnikant
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  2. Dinesh
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  3. Kamni
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  4. M.B. Deshmukh
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Rajnikant, Dinesh, Kamni et al. Synthesis and X-ray structure analysis of 2-acetylamino-benzoic acid. Journal of Chemical Crystallography 34, 471–475 (2004). https://doi.org/10.1023/B:JOCC.0000035389.59351.3a

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  • DOI: https://doi.org/10.1023/B:JOCC.0000035389.59351.3a

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