Abstract
The impurity contents of different silicon tetrafluoride samples (isotopically unmodified and enriched) are determined by optical emission spectroscopy with the preconcentration of nonvolatile impurities by distilling off SiF4 .
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REFERENCES
Kvaratskheli, Yu.K. and Sviderskii, M.F., Developments in Solar Energy Conversion at MINATOM, Konversiya Mashinostr., 1999, no. 3/4, pp. 44–48.
Bulanov, A.D., Balabanov, V.V., Pryakhin, D.A., and Troshin, O.Yu., Preparation and Fine Purification of SiF 4 and 28SiH4, Neorg.Mater., 2002, vol. 38, no. 3, pp. 35-361 [Inorg.Mater. (Engl. Transl.), vol. 38, no. 3, pp. 283–287].
Tarbeyev, Y.V., Kaliteyevsky, A.K., Sergeyev, V.I., et al., Scientific, Engineering, and Metrological Problems in Producing Pure Si-28 and Growing Single Crystals, Metrologia, 1994, vol. 31, no. 3, pp. 269–273.
Sanjurjo, A., Nanis, L., Sancier, K., et al., Silicon by Sodium Reduction of Silicon Tetrafluoride, J.Electrochem.Soc., 1981, vol. 128, no. 1, pp. 179–184.
Devyatykh, G.G., Shishov, V.N., Balabanov, V.V., et al., Determination of Impurities in the Form of Suspended Particles in Volatile Inorganic Hydrides, Zh.Anal.Khim., 1977, vol.32, pp. 1578–1582.
Devyatykh, G.G., Shishov, V.N., Pimenov, V.G., et al., Spectrochemical Determination of Metal Microimpurities in Extrapure Titanium Tetrachloride, Zh.Anal.Khim., 1978, vol. 33, pp. 464–467.
Shishov, V.N., Dryakhlova, I.A., Voronkova, T.V., and Loginov, A.V., Sources of Background Impurities in Analysis of High-Purity Silicon and Germanium Tetra-chlorides by Optical Emission Spectroscopy, Vysokochist.Veshchestva, 1988, no. 5, pp. 121–125.
Shishov, V.N., Spectrochemical Analysis of High-Purity Volatile Inorganic Hydrides, Halides, and Organoele-ment Compounds, Vysokochist.Veshchestva, 1990, no. 4, pp. 33–47.
Devyatykh, G.G., Pryakhin, D.A., Bulanov, A.D., et al., Phase Diagram of Silicon Tetrafluoride, Dokl.Akad.Nauk, 1999, vol. 364, no. 1, pp. 75–76.
Tanaka, K., Isomura, S., Kaetsu, H., et al., Gram-Order Preparation of 30 Si-Enriched Silica and Silicon Powders by Means of IRMPD of Disilicon Hexafluoride, Bull.Chem.Soc.Jpn., 1996, vol. 69, pp. 493–498.
Gaivoronskii, P.E. and Pimenov, V.G., Apparatus for Removing Nonvolatile Impurities from Liquids, Zavod.Lab., 1984, vol. 50, no. 6, pp. 20–21.
Shishov, V.N., Pimenov, V.G., and Gordeev, A.M., Use of the Cathodic Arc Plasma Effect for Lowering the Detection Limit of Optical Emission Spectroscopy, Vysokochist.Veshchestva, 1989, no. 4, pp. 214–219.
Zolotov, Yu.A. and Kuz'min, N.M., Kontsentrirovanie microelementov (Concentration of Microelements), Moscow: Khimiya, 1982, p. 13.
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Bulanov, A.D., Pimenov, V.G. Determination of Impurities in Monoisotopic Silicon Tetrafluoride. Inorganic Materials 40, 754–759 (2004). https://doi.org/10.1023/B:INMA.0000034777.13686.f8
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DOI: https://doi.org/10.1023/B:INMA.0000034777.13686.f8