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Formation of the Dinitro-3H-pyrazole Derivative of Cycloartemisiaketone Oxime

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Abstract

(3aR*,6aR*)-3,3,5,5-Tetramethyl-3a,6a-dinitro-3a,6a-dihydro-3H-cyclopentano[c]pyrazol-2-oxide was formed by reaction of cycloartemisiaketone oxime [4,4-dimethyl-2-(1-methylethylidene)cyclopentanone oxime] with AcOH and NaNO2 in CHCl3 solution. The structure was solved by x-ray structure analysis.

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Authors and Affiliations

  1. Institute of Phytochemistry, Ministry of Education and Science of the Republic of Kazakhstan, Republic of Kazakhstan, 470032, Karaganda, ul. Gazalieva 4

    E. M. Suleimenov, G. A. Atazhanova, A. T. Kulyyasov & S. M. Adekenov

  2. Novosibirsk Institute of Organic Chemistry, Siberian Division, Russian Academy of Sciences, 630090, Novosibirsk, pr. Akad. Lavrent'eva, 9

    V. A. Raldugin, I. Yu. Bagryanskaya, Yu. V. Gatilov & M. M. Shakirov

Authors
  1. E. M. Suleimenov
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  2. G. A. Atazhanova
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  3. A. T. Kulyyasov
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  4. V. A. Raldugin
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  5. I. Yu. Bagryanskaya
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  6. Yu. V. Gatilov
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  7. M. M. Shakirov
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  8. S. M. Adekenov
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Suleimenov, E.M., Atazhanova, G.A., Kulyyasov, A.T. et al. Formation of the Dinitro-3H-pyrazole Derivative of Cycloartemisiaketone Oxime. Chemistry of Natural Compounds 40, 134–136 (2004). https://doi.org/10.1023/B:CONC.0000033928.00722.fa

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  • DOI: https://doi.org/10.1023/B:CONC.0000033928.00722.fa

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