Abstract
The newderivative 5β-chloro-4α-methoxysantonin oximewasprepared from5β-chloro-4α-methoxysantonin by reaction with hydroxylamine hydrochloride in the presence of pyridine. The structure was established by IR, UV, and PMR spectroscopies.
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REFERENCES
B. H. B. Kwok, B. Koh, M. I. Ndubuisi, M. Elofsson, and C. M. Crews, Chem. Biol., 8/8, 759 (2001).
G. Blay, L. Cardona, B. Garcia, C. L. Garcia, and J. R. Pedro, Tetrahedron, 52, 31, 10507 (1996).
G. Blay, V. Bargues, L. Cardona, B. Garcia, and J. R. Pedro, Tetrahedron, 57, 31, 9719 (2001).
H. Takayanagi, H. Ogura, T. Brian, and T. B. H. McMurry, Bull. Chem. Soc. Jpn., 54, 4, 1259 (1981).
H. Takayanagi, H. Ogura, and T. B. H. McMurry, Chem. Pharm. Bull., 38, 3, 581 (1990).
H. Takayanagi, R. Irimajiri, and T. B. H. McMurry, Chem. Pharm. Bull., 39, 3, 780 (1991).
K. C. Engvild, Phytochemistry, 25, 4, 781 (1986).
A. V. Tkachev, Author's Abstract of a Doctoral Dissertation in Chemical Sciences, NIOKh, Russ. Acad. Sci., Novosibirsk (1996).
G. A. Atazhanova, A. T. Kulyyasov, V. A. Raldugin, A. D. Dembitskii, M. M. Shakirov, I. Yu. Bagryanskaya, Yu. V. Gatilov, S. M. Adekenov, and A. G. Tolstikov, Khim. Prir. Soedin., 121 (2000).
K. S. Rybalko, Natural Sesquiterpene Lactones [in Russian], Meditsina, Moscow (1978).
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Ivasenko, S.A., Kulyyasov, A.T. & Adekenov, S.M. Synthesis of 5 β-Chloro-4α-methoxysantonin Oxime. Chemistry of Natural Compounds 39, 573–574 (2003). https://doi.org/10.1023/B:CONC.0000018112.50820.81
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DOI: https://doi.org/10.1023/B:CONC.0000018112.50820.81