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Test Method for the Determination of Mercury(II) with Dithizone on the Solid Phase of a Fibrous Anion Exchanger

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Abstract

The sorption and determination of mercury(II) on the solid phase of a fibrous polyacrylonitrile material filled with the AV-17 anion exchanger is studied. Mercury is adsorbed in the form of the chloride complex from a solution with pH 5–7.5; it is determined on the solid phase by the reaction with dithizone either visually or by the measuring the color hue. A procedure for the test determination of mercury(II) has been developed and tested in the analysis of fresh natural waters by the added–found method. The detection limit is 0.02 mg/L. The time of analysis of 5 or 6 samples is no more than 15–20 min.

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Dedkova, V.P., Shvoeva, O.P. & Savvin, S.B. Test Method for the Determination of Mercury(II) with Dithizone on the Solid Phase of a Fibrous Anion Exchanger. Journal of Analytical Chemistry 59, 381–385 (2004). https://doi.org/10.1023/B:JANC.0000022793.59702.ab

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  • DOI: https://doi.org/10.1023/B:JANC.0000022793.59702.ab

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