Skip to main content
Log in

Dry Pressing Boehmite Gels for the Fabrication of Monolithic α-Al2O3

  • Published:
Journal of Sol-Gel Science and Technology Aims and scope Submit manuscript

Abstract

It is demonstrated that dense alpha alumina can be fabricated by pressing ethanol-dispersed, α-Al2O3 seeded boehmite. Green bodies were formed by uniaxially pressing either water or ethanol dispersed gel powder and then isostatically pressing the compacts at 280 MPa. Green microstructure and alumina densification are correlated with gel agglomerate size and dispersing medium. The ethanol-dispersed specimens showed better sinterability than the water-dispersed specimens, and sintered to more than 99% theoretical density at 1300°C. It is shown that softer gel agglomerates were obtained by alcohol dispersion and resulted in better green microstructure and higher sintered density.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. D.I. Matkin, W. Munro, and T.M. Valentine, J. Mater. Sci. 6, 974 (1971).

    Google Scholar 

  2. P.A. Badkar, J.E. Bailey, and H.A. Baker, in Sintering and Related Phenomena, edited by G.C. Kuczynski, Mater. Sci. Res. (Plenum, New York, 1973), vol. 6, p. 311.

    Google Scholar 

  3. P.F. Becher, J.H. Sommers, B.A. Bender, and B.A. MacFarlane, in Processing of Crystalline Ceramics, edited by H. Palmour IV, R.F. Davis, and T. Hare, Mater. Sci. Res. (Plenum, New York, 1978), vol. 11, p. 79.

    Google Scholar 

  4. B.E. Yoldas, J. Am. Ceram. Soc. 65, 387 (1982).

    Google Scholar 

  5. M. Kumagai and G.L. Messing, J. Am. Ceram. Soc. 68, 500 (1985).

    Google Scholar 

  6. Y. Suwa and R. Roy, Mater. Sci. & Eng. 83, 151 (1986).

    Google Scholar 

  7. E. Prouzet, D. Fargeot, and J.F. Baumard, J. Mater. Sci. Letter 9, 779 (1990).

    Google Scholar 

  8. J.L. McArdle and G.L. Messing, Adv. Ceram. Mater. 3, 387 (1988).

    Google Scholar 

  9. J.L. McArdle and G.L. Messing, J. Am. Ceram. Soc. 67, c-230 (1984).

    Google Scholar 

  10. M. Kumagai and G.L. Messing, J. Am. Ceram. Soc. 68, 500 (1985).

    Google Scholar 

  11. G.L. Messing and M. Kumagai, Am. Ceram. Soc. Bull. 73, 88 (1994).

    Google Scholar 

  12. G.W. Scherer, in Better Ceramics Through Chemistry II, edited by C.J. Brinker, D.E. Clark, and D.R. Ulrich (Materials Research Society, Pittsburgh, PA, 1986), p. 225.

    Google Scholar 

  13. A.F.M. Leenaars, L. Keizer, and A.J. Burggraaf, J. Mater. Sci. 19, 1077 (1984).

    Google Scholar 

  14. A.C. Pierre and D.R. Uhlmann, in Better Ceramics Through Chemistry II, edited by C.J. Brinker, D.E. Clark, and D.R. Ulrich (Materials Research Society, Pittsburgh, PA, 1986), p. 481.

    Google Scholar 

  15. J.J. Lannutti and D.E. Clark, Ceramics International. 11, 91 (1985).

    Google Scholar 

  16. D.S. Horn and G.L. Messing, J. Am. Ceram. Soc. 72, 1719 (1989).

    Google Scholar 

  17. T.V. Mani, P.K. Pillai, A.D. Damodaran, and K.G.K. Warrier, Materials Letters 19, 237 (1994).

    Google Scholar 

  18. A. Roosen and H. Hausner, Adv. Ceram. Mater. 3, 131 (1988).

    Google Scholar 

  19. H.K. Varma, T.V. Mani, A.D. Damodaran, K.G. Warrier, and U. Balachandran, J. Am. Ceram. Soc. 77, 1597 (1994).

    Google Scholar 

  20. M.F.L. Johnson and J. Mooi, Journal of Catalysis 10, 342 (1968).

    Google Scholar 

  21. M.J. Readey, R.R. Lee, J.W. Halloran, and A.H. Heuer, J. Am. Ceram. Soc. 73, 1499 (1990).

    Google Scholar 

  22. A. Roosen and H.K. Bowen, J. Am. Ceram. Soc. 71, 970 (1988).

    Google Scholar 

  23. J.W. Halloran, in Ultrastructure Processing of Ceramics, Glass, and Composites, edited by L.L. Hench and D.R. Ulrich (Wiley, New York, 1984), p. 404.

    Google Scholar 

Download references

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Kwon, S., Messing, G.L. Dry Pressing Boehmite Gels for the Fabrication of Monolithic α-Al2O3 . Journal of Sol-Gel Science and Technology 9, 53–64 (1997). https://doi.org/10.1023/A:1026460323483

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/A:1026460323483

Navigation