Skip to main content
SpringerLink
Log in

Sol-Gel Synthesis of Monodispersed SiO2 Nanoparticles in the Presence of Organic Amines

  • Published:
Russian Journal of Applied Chemistry Aims and scope Submit manuscript

Abstract

Preparation of monodispersed SiO2 nanoparticles of varied size by hydrolysis of tetramethoxysilane and polycondensation of the hydrolysis products was studied as influenced by the basicity and nucleophilicity of organic amines.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Stöber, W. and Fink, A., J. Colloid Interface Sci., 1968, vol. 26, pp. 62-69.

    Google Scholar 

  2. Petrovskii, G.T., Shashkin V.S., Yakhkind, A.K., Fiz. Khim. Stekla, 1997, vol. 23, no. 1, pp. 43-53.

    Google Scholar 

  3. So, J.-H., Oh, M.-H., Lee, J.-D., and Yang, S.-M., J. Chem. Eng. Jpn., 2001, vol. 34, no. 2, pp. 262-268.

    Google Scholar 

  4. Efremov, I.F., Periodicheskie kolloidnye struktury (Periodical Colloid Structures), Leningrad: Khimiya, 1971.

    Google Scholar 

  5. Hunter, R.J., Foundations of Colloid Science, Oxford: Univ. Press, 2001.

    Google Scholar 

  6. Okubo, T. And Ishiki, H., J. Colloid. Interface Sci., 1999, vol. 211, p. 151-159.

    Google Scholar 

  7. Bogush, G.H., Tracy, M.A., and Zukoski, C.F., J. Non-Cryst. Solids, 1988, vol. 104, pp. 95-106.

    Google Scholar 

  8. So, Jae-Hyun, Yang, Seung-Man, Kim, C., and Hyn, J.C., Colloids Surf. A: Physicochem. Eng. Aspects, 2001, vol. 190, pp. 89-98.

    Google Scholar 

  9. Sung Kyoo Park, Ki Do Kim, and Hee Taik Kim, Colloids Surf. A: Physicochem. Eng. Aspects, 2002, vol. 197, pp. 7-17.

    Google Scholar 

  10. Brinker, C.I. and Scherer, G.W., Sol-Gel Science, New York: Academic, 1990.

    Google Scholar 

  11. Pope, E.J.A. and Mackenzie, J.D., J. Non-Cryst. Solids, 1986, vol. 87, pp. 185-198.

    Google Scholar 

  12. Corriu, R.J.P. and Young, J.C., The Chemistry of Organic Silicon Compounds, Patai, S. and Rappoport, Z., Eds., New York: Wiley, 1989, ch. 20, pp. 1241-1288.

    Google Scholar 

  13. Carey, F.A. and Sundberg, R.J., Advanced Organic Chemistry, Part A: Structure and Mechanisms, New York: Plenum, 1977.

    Google Scholar 

  14. Aldrich Catalog Handbook of Fine Chemicals, Sigma-Aldrich, 2000.

  15. Beilstein Handbook of Organic Chemistry: Fifth Suppl. Ser., Berlin: Springer, 1989, vol. 20, part 6.

  16. Perrin, D.D., Dissociation Constants of Organic Bases in Aqueous Solutions, London: Butterworths, 1965.

    Google Scholar 

  17. Klein, L.C., Ann. Rev. Mater. Sci., 1985, vol. 15, pp. 227-248.

    Google Scholar 

  18. Iler, R.K., The Chemistry of Silica, New York: Wiley-Interscience, 1979.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Institute of Silicate Chemistry, Russian Academy of Sciences, St. Petersburg, Russia

    N. N. Khimich, Yu. V. Zvyagil'skaya, A. N. Zhukov & O. G. Us'yarov

  2. St. Petersburg State University, St. Petersburg, Russia

    N. N. Khimich, Yu. V. Zvyagil'skaya, A. N. Zhukov & O. G. Us'yarov

Authors
  1. N. N. Khimich
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Yu. V. Zvyagil'skaya
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. A. N. Zhukov
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. O. G. Us'yarov
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Khimich, N.N., Zvyagil'skaya, Y.V., Zhukov, A.N. et al. Sol-Gel Synthesis of Monodispersed SiO2 Nanoparticles in the Presence of Organic Amines. Russian Journal of Applied Chemistry 76, 875–878 (2003). https://doi.org/10.1023/A:1026351321023

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/A:1026351321023

Keywords

Search

Navigation