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Voltammetric Determination of Tin(II) and Iron(II) on Mechanically Renewed Graphite Electrode in Tin-Plating Electrolyte

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Abstract

The analytical properties of the cathodic peak of tin(II) reduction and the anodic peak of iron(II) oxidation on a graphite electrode were studied with the electrode surface mechanically renewed directly in a solution before applying a potential in each measurement. The influence of the organic components of the phenolsulfonic tin-plating electrolyte on the cathodic current of tin(II) reduction and anodic current of iron(II) oxidation was studied. A dc voltammetric method was proposed for determining tin(II) directly in the phenolsulfonic tin-plating electrolyte, and iron(II) after the electrolyte is diluted tenfold with a 0.5M H2SO4 supporting solution.

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Authors and Affiliations

  1. Institute of Solid-State Chemistry and Mechanochemistry, Siberian Division, Russian Academy of Sciences, Novosibirsk, Russia

    L. I. Skvortsova & A. Zh. Medvedev

Authors
  1. L. I. Skvortsova
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  2. A. Zh. Medvedev
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Skvortsova, L.I., Medvedev, A.Z. Voltammetric Determination of Tin(II) and Iron(II) on Mechanically Renewed Graphite Electrode in Tin-Plating Electrolyte. Russian Journal of Applied Chemistry 76, 912–916 (2003). https://doi.org/10.1023/A:1026319808727

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  • DOI: https://doi.org/10.1023/A:1026319808727

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