Abstract
Atmospheric aerosols are generally collected on filters according to the International Monitoring System (IMS) designed in the Comprehensive Nuclear-Test-Ban Treaty (CTBT). More information could be revealed when the filter sample is pretreated rather than measured directly by g-ray spectrometer. Microwave-assisted extraction (MAE) is a suitable method that gives higher recoveries of elements from glass fibrous filters under different conditions. The results indicate that the MAE is a highly efficient and robust method for the treatment of glass fibrous filter samples. The recoveries of potential fission products from glass fibrous filter samples by microwave-assisted extraction meet the efficiency of the extraction by both aqua regia and 2% HCl.
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References
D. E. Kimbrough, I. H. 'Mel'suffet, Analyst, 121 (1996) 309.
S. L. Harper, J. F. Walling, D. M. Holland, L. J. Pranger, Anal. Chem., 55 (1983) 1553.
J. Nieuwenhuize, C. H. Poly-Vos, A. H. van den Akker, W. van Delft, Analyst, 116 (1991) 347.
Compendium Method IO-3.1, Selection, Preparation and Extraction of Filter Material, in: Compendium of Methods for the Determination of Inorganic Compounds in Ambient Air, Updated:1999-9-1, U.S. Environmental Protection Agency, Cincinnati, 1999.
SW-846 EPA Method 3051A, Microwave Assisted Acid Digestion of Sediments, Sludges Soils, and Oils, in: Test Methods for Evaluating Solid Waste, Revision 1, Updated: Jan. 1998, US Environmental Protection Agency, Washington DC, 1998.
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Dong-Mei, L., Li-Xing, Z., Xu-Hui, W. et al. Microwave-assisted extraction of metal elements from glass fibrous filters for aerosol sampling. Journal of Radioanalytical and Nuclear Chemistry 258, 195–197 (2003). https://doi.org/10.1023/A:1026251318823
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DOI: https://doi.org/10.1023/A:1026251318823