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1H and 13C NMR Study of the Structure of Alkylthio Enyne Alcohols and Glycols

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Abstract

Steric structure of some alkylthio enyne alcohols and glycols was determined by 1H and 13C NMR spectroscopy. Analysis of cross peaks in the 2M NOESY spectra showed that the double bond in these compounds has Z configuration. Criteria were found which indicate the position of the hydroxy-containing substituent with respect to the triple or double bond.

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Authors and Affiliations

  1. Irkutsk Institute of Chemistry, Siberian Division, Russian Academy of Sciences, ul. Favorskogo 1, Irkutsk, 664033, Russia

    A. V. Afonin & K. A. Volkova

  2. Irkutsk State Technical University, Irkutsk, Russia

    S. Yu. Kuznetsova, I. A. Ushakov, V. K. Voronov, E. I. Basina & A. N. Volkov

Authors
  1. A. V. Afonin
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  2. S. Yu. Kuznetsova
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  3. I. A. Ushakov
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  4. V. K. Voronov
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  5. E. I. Basina
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  6. A. N. Volkov
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  7. K. A. Volkova
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Afonin, A.V., Kuznetsova, S.Y., Ushakov, I.A. et al. 1H and 13C NMR Study of the Structure of Alkylthio Enyne Alcohols and Glycols. Russian Journal of Organic Chemistry 38, 1437–1439 (2002). https://doi.org/10.1023/A:1022535901177

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  • DOI: https://doi.org/10.1023/A:1022535901177

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