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Characterisation of different inulin samples by DSC: Influence of polymerisation degree on melting temperature

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Abstract

Melting behaviour of powder inulin has been studied by differential scanning calorimetry. DSC curves show two endothermic peaks, relative to water elimination and to inulin melting, respectively. The second peak is dependent on inulin type and a shift to a higher temperature is observed with increasing average polymerisation degree (DP) of the sample. For similar crystallinity index, linear relations have been underlined and so predicting inulin mean DP can be done by DSC analysis. The study shows that a relatively high heating rate (25°C min−1) can be used and brings a supplementary interest by an important reduction of analysis time.

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References

  1. L. De Leenheer and H. Hoebregs, Starch/Stärke, 46 (1994) 193.

    Google Scholar 

  2. C. Blecker, C. Fougnies, J.-C. Van Herck, J.-P. Chevalier and M. Paquot, Int. J. Biol. Macromol., 50 (2002) 1602.

    Google Scholar 

  3. M. Roberfroid and N. Delzenne, Annu. Rev. Nutr., 18 (1998) 117.

    Google Scholar 

  4. C. Blecker, J.-P. Chevalier, J.-C. Van Herck, C. Fougnies, C. Deroanne and M. Paquot, Recent Res. Develop. Agric. Food Chem., 5 (2002) 125.

    Google Scholar 

  5. W. Hinrichs, M. Prinsen and H. Frijlink, Int. J. Pharm., 215 (2001) 163.

    Google Scholar 

  6. Y. Kim, M. Faqih and S. Wang, Carbohydr. Polym., 46 (2001) 135.

    Google Scholar 

  7. C. Hébette, J. Delcour, M. Koch, K. Booten, R. Kleppinger, N. Mischenko and H. Reynaers, Carbohydr. Res., 310 (1998) 65.

    Google Scholar 

  8. A. Heyer, B. Schroeer, S. Radosta, D. Wolff, S. Czapla and J. Springer, Carbohydr. Res., 313 (1998) 165.

    Google Scholar 

  9. J. Zimeri and J. Kokini, Carbohydr. Polym., 48 (2002) 229.

    Google Scholar 

  10. L. Schaller-Povolny, D. Smith and T. Labuza, Int. J. Food Prop., 3 (2000) 173.

    Google Scholar 

  11. C. Blecker, H. Razafindralambo, J.-P. Chevalier, B. Wathelet, C. Deroanne and M. Paquot, World Intellectual Property Organisation WO 0104161 (2001).

  12. J. Timmermans, M. Van Leeuwen, H. Tourmois, D. de Wit and J. Vliegenthart, J. Carbohydr. Chem., 13 (1994) 881.

    Google Scholar 

  13. S.-I. Kang, Ph.D. Thesis, Seoul National University, Korea 1999.

  14. R. Marchessault, T. Bleha, Y. Deslandes and J.-F. Revol, Can. J. Chem., 58 (1980) 2415.

    Google Scholar 

  15. I. André, J. Putaux, H. Chanzy, F. Taravel, J. Timmermans and D. de Wit, Int. J. Biol. Macromol., 18 (1996) 195.

    Google Scholar 

  16. I. André, K. Mazeau, I. Tvaroska, J.-L. Putaux, W. Winter, F. Taravel and H. Chanzy, Macromolecules, 29 (1996) 4626.

    Google Scholar 

  17. D. C. Bassett, Principles of polymer morphology, Cambridge University Press, Cambridge 1981, p. 69.

    Google Scholar 

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Correspondence to C. Blecker.

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Blecker, C., Chevalier, JP., Fougnies, C. et al. Characterisation of different inulin samples by DSC: Influence of polymerisation degree on melting temperature. Journal of Thermal Analysis and Calorimetry 71, 215–224 (2003). https://doi.org/10.1023/A:1022238905962

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  • DOI: https://doi.org/10.1023/A:1022238905962

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