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Fabrication of Monolithic Ti3SiC2 Ceramic Through Reactive Sintering of Ti/Si/2TiC

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Journal of Materials Synthesis and Processing

Abstract

Fabrication of monolithic Ti3SiC2 has been investigated through the route of reactive sintering of Ti/Si/2TiC mixtures. Significant phase differences existed between the surface and the interior of as-synthesized products due to the evaporation of Si during the reaction process. The use of a 3Ti/SiC/C mixture as a powder bed could control the evaporation of Si and develop monolithic Ti3SiC2. A reaction model for the formation of Ti3SiC2 in the Ti/Si/2TiC system is discussed.

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Authors and Affiliations

  1. Laboratory of Special Ceramics & P/M, University of Science & Technology, Beijing, Beijing, 100083, P.R. China

    J. T. Li

  2. Osaka University, 567, Osaka, Japan

    J. T. Li & Y. Miyamoto

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  1. J. T. Li
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  2. Y. Miyamoto
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Li, J.T., Miyamoto, Y. Fabrication of Monolithic Ti3SiC2 Ceramic Through Reactive Sintering of Ti/Si/2TiC. Journal of Materials Synthesis and Processing 7, 91–96 (1999). https://doi.org/10.1023/A:1021865613357

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  • DOI: https://doi.org/10.1023/A:1021865613357

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