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High-resolution and cross-polarization magic angle spinning NMR studies of tricarbonylchromium complexes with polycyclic aromatic ligands

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Abstract

The strategy of investigation of the structures and transformations of organometallic compounds by high-resolution NMR spectroscopy in solutions and in the solid state (cross-polarization magic angle spinning NMR) was considered in relation to tricarbonylchromium complexes with polycyclic aromatic ligands.

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References

  1. Advanced Applications of NMR to Organometallic Chemistry (Physical Organometallic Chemistry), Vol. 1, Eds. M. Gielen, R. Willem, and B. Wrackmeyer, J. Wiley, New York, 1996.

    Google Scholar 

  2. B. E. Mann, Chem. Soc. Rev., 1986, 15, 167.

    Google Scholar 

  3. B. E. Mann, in Comprehensive Organometallic Chemistry, Eds. G. Wilkinson, F. G. A. Stone, and E. W. Abel, Pergamon Press, Oxford, 1982, 3, Ch. 20, 89.

    Google Scholar 

  4. K. Schlögl, A. Werner, and M. Widhalm, J. Chem. Soc., Perkin Trans. 1, 1983, 1731.

  5. NMR Techniques in Catalysis, Eds. A. Bell and A. Pines, Marcel Dekker, New York, 1994.

    Google Scholar 

  6. F. A. Cotton, in Dynamic Nuclear Magnetic Resonance, Eds. L. M. Jackman and F. A. Cotton, Academic Press, New York, 1975, Ch. 10, 377.

    Google Scholar 

  7. Ch. Elschenbroich and A. Salzer, Organometallics, an Introduction, 2nd ed., Wiley-VCH Verlag, Weinheim (Germany), 1992.

    Google Scholar 

  8. Yu. N. Luzikov, Yu. F. Oprunenko, Yu. A. Ustynyuk, and N. A. Ustynyuk, J. Organomet. Chem., 1982, 231, 137.

    Google Scholar 

  9. N. S. Hush, J. Am. Chem. Soc., 1997, 119, 1717.

    Google Scholar 

  10. R. H. Crabtree and D. G. Hamilton, J. Am. Chem. Soc., 1986, 108, 312.

    Google Scholar 

  11. B. E. Mann, J. Chem. Soc., Dalton Trans., 1984, 2027.

  12. R. A. Bell and J. K. M. Saunders, Can. J. Chem., 1970, 48, 1114.

    Google Scholar 

  13. Yu. F. Oprunenko, S. G. Malyugina, Yu. A. Ustynyuk, N. A. Ustynyuk, and D. N. Kravtsov, J. Organomet. Chem., 1988, 338, 387.

    Google Scholar 

  14. N. A. Ustynyuk, L. N. Novikova, V. K. Bel'skii, Yu. F. Oprunenko, S. G. Malyugina, and Yu. A. Ustynyuk, J. Organomet. Chem., 1985, 294, 31.

    Google Scholar 

  15. F. McGlinchey, F. A. Roberts, and P. N. Dodge, J. Am. Chem. Soc., 1993, 115, 7275.

    Google Scholar 

  16. B. E. Mann, Adv. Organomet. Chem., 1988, 28, 397.

    Google Scholar 

  17. I. D. Gridnev, M. E. Gursky, and Yu. N. Bubnov, Organometallics, 1996, 15, 3696.

    Google Scholar 

  18. R. K. Harris, Nuclear Magnetic Resonance Spectroscopy, Pitman, London, 1983.

    Google Scholar 

  19. C. S. Yannoni, Acc. Chem. Res., 1982, 15, 201.

    Google Scholar 

  20. R. Benn, R. Mynott, I. Topalovic, and F. Scott, Organometallics, 1989, 8, 2299.

    Google Scholar 

  21. A. Stanger, Organometallics, 1991, 10, 2979.

    Google Scholar 

  22. G. B. Nagy, Multinuclear Magnetic Resonance in Liquids and Solids-Chemical Applications, Eds. B. Granger and R. K. Harris, NATO ASI Ser. C, Springer Verlag, Berlin, 1990, 322; 371.

    Google Scholar 

  23. R. Csuk, B. I. Glänzer, and A. Fürstner, Adv. Organomet. Chem., 1988, 28, 85.

    Google Scholar 

  24. H. Estrade-Schwarzkopf and K. H. Müller, J. Phys. Chem., 1985, 89, 97.

    Google Scholar 

  25. P. Styles and N. Soffe, J. Magn. Reson., 1984, 50, 397.

    Google Scholar 

  26. G. Engelhardt and D. Michel, High Resolution Solid State NMR of Silicates and Zeolites, J. Wiley, Chichester, 1987.

    Google Scholar 

  27. P. G. Gassman and P. A. Deck, Organometallics, 1994, 13, 1934.

    Google Scholar 

  28. J. A. Ramsden, C. M. Garner, and J. A. Gladysz, Organometallics, 1991, 10, 1631.

    Google Scholar 

  29. E. Yashima, C. Yamamoto, and Y. Okamoto, J. Am. Chem. Soc., 1996, 118, 4036.

    Google Scholar 

  30. D. J. States, R. A. Habekorn, and D. J. Ruben, J. Magn. Reson., 1982, 48, 286.

    Google Scholar 

  31. M. Rance, G. Bodenhausen, G. Wagner, K. Wütrich, and R. R. Ernst, J. Magn. Reson., 1985, 62, 497.

    Google Scholar 

  32. G. A. Morris and K. J. Smith, J. Magn. Reson., 1985, 65, 506.

    Google Scholar 

  33. G. A. Morris and R. Freeman, J. Am. Chem. Soc., 1979, 101, 760.

    Google Scholar 

  34. Yu. F. Oprunenko, Sc.D. Thesis (Chem.), Moscow State University, Moscow, 1999 (in Russian).

  35. D. Neuhaus and M. P. Williamson, The Nuclear Overhauser Effect in Structural and Conformational Analysis, VCH Edition, Weinheim, 1989.

    Google Scholar 

  36. K. E. Kövér and G. Batta, J. Am. Chem. Soc., 1985, 107, 5829.

    Google Scholar 

  37. J. K. M. Saunders and J. D. Mersh, Prog. Nucl. Magn. Reson. Spectrosc., 1982, 15, 353.

    Google Scholar 

  38. Yu. F. Oprunenko, N. G. Akhmedov, S. G. Malyugina, V. I. Mstislavsky, V. A. Roznyatovsky, D. N. Laikov, Yu. A. Ustynyuk, and N. A. Ustynyuk, J. Organomet. Chem., 1999, 583, 136.

    Google Scholar 

  39. W. J. Bland, R. Davis, and J. L. A. Durrant, J. Organomet. Chem., 1984, 234, C20.

    Google Scholar 

  40. Yu. A. Ustynyuk, O. I. Trifonova, and Yu. F. Oprunenko, Metalloorgan. Khim., 1993, 6, 654 [Organomet. Chem. USSR, 1993, 6 (Engl. Transl.)].

    Google Scholar 

  41. Yu. F. Oprunenko, I. A. Shaposhnikova, and Yu. A. Ustynyuk, Metalloorgan. Khim., 1991, 4, 684 [Organomet. Chem. USSR, 1991, 4 (Engl. Transl.)].

    Google Scholar 

  42. Yu. F. Oprunenko, S. G. Malyugina, O. Ya. Babushkina, Yu. A. Ustynyuk, P. N. Nesterenko, N. A. Ustynyuk, D. N. Kravtsov, and V. A Piven´, Metalloorgan. Khim., 1988, 1, 384 [Organomet. Chem. USSR, 1988, 1 (Engl. Transl.)].

    Google Scholar 

  43. Yu. F. Oprunenko, S. G. Malyugina, O. Ya. Babushkina, Yu. A. Ustynyuk, N. A. Ustynyuk, and D. N. Kravtsov, Metalloorgan. Khim., 1989, 2, 599 [Organomet. Chem. USSR, 1989, 2 (Engl. Transl.)].

    Google Scholar 

  44. M. Rance, O. W. Sorensen, G. Bodenhausen, G. Wagner, R. R. Ernst, and R. Wütrich, Biochem. Biophys. Res. Commun., 1983, 117, 479.

    Google Scholar 

  45. D. J. States, R. A. Haberkorn, and D. J. Ruben, J. Magn. Reson., 1982, 48, 286.

    Google Scholar 

  46. R. R. Ernst, G. Bodenhausen, and A. Wokaun, Principles of Nuclear Magnetic Resonance in One and Two Dimensions, Oxford University, Oxford, 1987.

    Google Scholar 

  47. J. M. Lamarche, J. Vefrel, and B. Laude, Spectrochim. Acta, A, 1979, 35, 673.

    Google Scholar 

  48. W. R. Jackson and T. R. B. Mitchell, J. Chem. Soc., B, 1969, 1228.

  49. B. Caro, E. Gentric, D. Grandjean, and G. Jaouen, Tetrahedron Lett., 1978, 3009.

  50. D. E. F. Gracey, W. R. Jackson, C. H. McMullen, and N. Thompson, J. Chem. Soc., B, 1969, 2197.

  51. R. G. Sutherland, W. J. Pannekoek, and C. C. Lee, Can. J. Chem., 1978, 56, 1782.

    Google Scholar 

  52. E. M. Engler and P. Lazlo, J. Am. Chem. Soc., 1971, 93, 1317.

    Google Scholar 

  53. N. A. Ustynyuk, L. N. Novikova, V. K. Bel´skii, Yu. F. Oprunenko, S. G. Malyugina, O. I. Trifonova, and Yu. A. Ustynyuk, J. Organomet. Chem., 1985, 294, 31.

    Google Scholar 

  54. D. E. F. Gracey, W. E. Jackson, W. B. Jennings, S. R. Rehninson, and R. Span, J. Chem. Soc., B, 1969, 1210.

  55. A. C. Sievert and E. I. Muetterties, Inorg. Chem., 1981, 20, 2278.

    Google Scholar 

  56. B. M. Bandara, A. J. Birch, and W. D. Raverty, J. Chem. Soc., Perkin Trans. 1, 1982, 1945.

  57. L. A. Paquette and R. Gree, J. Organomet. Chem., 1978, 146, 319.

    Google Scholar 

  58. N. A. Ustynyuk, L. N. Novikova, Yu. F. Oprunenko, S. G. Malyugina, and Yu. A. Ustynyuk, J. Organomet. Chem., 1984, 277, 75.

    Google Scholar 

  59. T. G. Traylor and M. J. Goldberg, Organometallics, 1987, 6, 2531.

    Google Scholar 

  60. B. E. Hanson, in Advances in Dynamic Stereochemistry, Ed. M. Gielen, Freund, London, 1985, 89.

    Google Scholar 

  61. G. W. Wagner and B. E. Hanson, Inorg. Chem., 1987, 26, 2019.

    Google Scholar 

  62. R. Benn, R. Mynott, I. Topalovic, and F. Scott, Organometallics, 1989, 8, 2299.

    Google Scholar 

  63. A. Stanger, Organometallics, 1991, 10, 2979.

    Google Scholar 

  64. A. E. Aliev, K. D. M. Harris, F. Guillaume, and P. J. Barrie, J. Chem. Soc., Dalton Trans., 1994, 3193.

  65. P. J. Barrie, Ch. A. Mitsopoulou, and E. W. Randall, J. Chem. Soc., Dalton Trans., 1995, 2125.

  66. P. J. Barrie, Ch. A. Mitsopoulou, M. Motevalli, and E. Randall, J. Chem. Soc., Dalton Trans., 1997, 353.

  67. Yu. Oprunenko, M. Ebener, G. von Fircks, and H. Guenther, XV Intern. Conf. on Organometallic Chemistry, Book of Abstrs., Warsaw, 1992, 84.

  68. J. S. Opella and M. H. Frey, J. Am. Chem. Soc., 1979, 101, 5854.

    Google Scholar 

  69. R. D. Rogers, J. L. Atwood, T. A. Albright, W. A. Lee, and M. D. Rausch, Organometallics, 1984, 3, 263.

    Google Scholar 

  70. M. J. McGlinchey, Adv. Organomet. Chem., 1992, 14, 285.

    Google Scholar 

  71. M. Nambu, D. L. Mohler, K. Hardcastle, K. K. Baldridge, and J. S. Siegel, J. Am. Chem. Soc., 1993, 115, 6138.

    Google Scholar 

  72. H. Günther, NMR-Spektroskopie, G. Thieme, Stuttgart, 1992.

    Google Scholar 

  73. V. I. Mstislavskii, Ph.D. Thesis (Physics and Mathematics), Moscow State University, Moscow, 1985 (in Russian).

  74. Yu. F. Oprunenko, A. S. Batsanov, S. G. Malyugina, M. D. Reshetova, N. A. Ustynyuk, and Yu. A. Ustynyuk, Organometallics, 1994, 13, 2284.

    Google Scholar 

  75. P. E. Baikie and O. S. Mills, J. Chem. Soc., A, 1969, 328.

  76. D. Braga, Chem. Rev., 1992, 92, 663.

    Google Scholar 

  77. V. Kunz and W. Nowacki, Helv. Chim. Acta, 1967, 50, 1052.

    Google Scholar 

  78. H. Pfeifer, W. Meiler, and D. Deininger, Ann. Rep. NMR Spectrosc., 1983, 15, 291.

    Google Scholar 

  79. M. Ebener, G. von Fircks, and H. Günther, Helv. Chim. Acta, 1991, 74, 1296.

    Google Scholar 

  80. P. Jackson and R. K. Harris, Magn. Reson. Chem., 1988, 26, 1003.

    Google Scholar 

  81. C. R. Anderson, M. A. Jarema, M. J. Shapiro, J. P. Stokes, and M. Ziliox, J. Org. Chem., 1995, 60, 2650.

    Google Scholar 

  82. M. Ebener, V. Francke, and H. Günther, Fresenius J. Anal. Chem., 1997, 357, 505.

    Google Scholar 

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  1. Department of Chemistry, M. V. Lomonosov Moscow State University, Leninskie Gory, 119899, Moscow, Russian Federation

    Yu. F. Oprunenko

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Oprunenko, Y.F. High-resolution and cross-polarization magic angle spinning NMR studies of tricarbonylchromium complexes with polycyclic aromatic ligands. Russian Chemical Bulletin 51, 907–929 (2002). https://doi.org/10.1023/A:1019629929837

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