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Synthesis and evaluation of various layered octacalcium phosphates by wet-chemical processing

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Abstract

Octacalcium phosphate was synthesized by hydrolysis of α-tricalcium phosphate through a wet-chemical processing. Using the same wet-chemical processing in presence of various succinate ions, the preparation of some complexed octacalcium phosphates was attempted. The products were examined by X-ray diffraction method. These complexed octacalcium phosphates intercalated with succinic acid, L-asparatic acid, and methyl succinic acid showed an expanded basal spacing in the octacalcium phosphate unit cell dimensions. The microstructure was observed by scanning and transmission electron microscopy. © 2001 Kluwer Academic Publishers

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Authors and Affiliations

  1. Kyoto Institute of Technology, Gosho-kaido-cho, Matsugasaki,Sakyo-ku, Kyoto, 606-8585, Japan

    A. Nakahira & S. Aoki

  2. Osaka Sangyo University, 3-1-1 Nakagaito, Daito, Osaka, 574-8530, Japan

    K. Sakamoto

  3. ISIR, Osaka University, 8-1 Mihogaoka, Ibaraki, 567-0047, Japan

    S. Yamaguchi

Authors
  1. A. Nakahira
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  2. S. Aoki
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  3. K. Sakamoto
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  4. S. Yamaguchi
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Nakahira, A., Aoki, S., Sakamoto, K. et al. Synthesis and evaluation of various layered octacalcium phosphates by wet-chemical processing. Journal of Materials Science: Materials in Medicine 12, 793–800 (2001). https://doi.org/10.1023/A:1017968818168

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  • DOI: https://doi.org/10.1023/A:1017968818168

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