Abstract
The procedures of production of mononitrochlorobenzene by nitration with 75-97% nitric acid with the yield of the target product of 97.5% were developed. A procedure of precipitation of crystalline p-nitrochlorobenzene from the reaction mixture without additional purification was proposed.
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Veretennikov, E.A., Lebedev, B.A. & Tselinskii, I.V. Nitration of Chlorobenzene with Nitric Acid in a Continuous Installation. Russian Journal of Applied Chemistry 74, 1872–1876 (2001). https://doi.org/10.1023/A:1014840627266
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DOI: https://doi.org/10.1023/A:1014840627266