Abstract
A principle is presented for reproducing the unit of combustion energy, the joule, on the GÉT 16-96 State Primary Standard, which is based on using high-purity benzoic acid grade K-1. Metrological characteristics are given for various types of benzoic acid produced in various countries and used in combustion calorimetry. A comparison is made of the combustion energies for Russian K-3 benzoic acid and American 39i, which have been obtained with a GÉT 16-96.
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References
GOST 8.026-96. The State System of Measurements: The State Test Scheme for Means of Measuring Combustion Energy and Specific Combustion Energy Combustion Calorimeters) [in Russian].
E. N. Korchagina and Yu. I. Aleksandrov, Izmer. Tekh., No. 5, 46 (1992).
Intern. Un. Pure and Applied Chem., Proc. Sec. Intern. Conf. Chem., Brussels (1921), pp. 26, 48, and 94.
E. F. G. Herington (ed.), “Recommended reference materials for realization of physicochemical properties,” Pure and Appl. Chem., 40, No. 3, 437 (1974).
B. N. Oleinik, Precision Calorimetry [in Russian], Izd. Standartov, Moscow (1973).
GSSSD 50-83, Benzoic Acid: Combustion Energy [in Russian].
Yu. I. Aleksandrov, V. F. Yushkevich, and G. A. Novikov, Vysokochist. Veshch., No. 6, 99 (1987).
Yu. I. Aleksandrov et al., Authors' Certificate 1065 404 USSR, Otkryt. Izobret., No. 1 (1984).
Yu. I. Aleksandrov et al., Authors' Certificate 1535 565 USSR, Otkryt. Izobret., No. 2 (1990).
Yu. I. Aleksandrov et al., Authors' Certificate 1604 866 USSR, Otkryt. Izobret., No. 41 (1990).
Yu. I. Aleksandrov, V. P. Varganov, and V. M. Samarina, Making and Analyzing Pure Substances: Intercollegiate Scientific Paper Collection from Gor'kii State University [in Russian], Gor'kii (1986), p. 84.
Yu. I. Aleksandrov et al., Physicochemical Analysis Methods: Intercollegiate Scientific Paper Collection from Gor'kii State University [in Russian], Gor'kii (1986), p. 95.
Yu. I. Aleksandrov et al., High-Purity Substances, 4, No. 1, 150 (1990).
Yu. I. Aleksandrov, V. I. Belyakov, and V. P. Varganov, Intercollegiate Scientific Paper Collection from Gor'kii State University [in Russian], Gor'kii (2000).
P. A. O'Hare, G. A. Hope, and G. M. Beck, J. Chem. Thermodyn., 25, No. 7, 918 (1993).
A. Carson et al., J. Chem. Thermodyn., 25, No. 2, 261–269, 229–235 (1993).
M. A. Ribeiro da Silva et al., ibid., 25, No. 5, 579–590 (1993).
M. A. Ribeiro da Silva, J. M. Consalves, and G. Pilcher, ibid., 29, No. 3, 253–260, 295–303 (1997).
Li Shaofeng et al., ibid., 22, No. 3, 319–320 (1990).
GOST 8.381-80, The State System of Measurements: Standards: Methods of Expressing Errors [in Russian].
Guide to the Expression of Uncertainty in Measurement, First Edition, ISO, Switzerland (1993).
MI 2552-99, The State System of Measurements: Using the Guide to the Expression of Uncertainty in Measurement [in Russian].
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Korchagina, E.N. Metrological Characteristics of K-1 and K-3 Reference Benzoic Acids. Measurement Techniques 44, 1138–1142 (2001). https://doi.org/10.1023/A:1014021519763
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DOI: https://doi.org/10.1023/A:1014021519763