Skip to main content
Log in

ZrO2 and Cu/ZrO2 Sol-Gel Synthesis in Presence of Microwave Irradiation

  • Published:
Journal of Sol-Gel Science and Technology Aims and scope Submit manuscript

Abstract

The sol-gel technique with a microwave irradiation was used to synthesize ZrO2 and Cu/ZrO2 solids at various pH values and hydrolysis catalysts. Microwave irradiation induces ZrO2 tetragonal phase formation at almost any pH. The copper was bonded through oxygen bonds to the zirconia lattice. The introduction of copper favored the support acidity.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. K.T. Miller, C.J. Chan, M.G. Cain, and F. Lange, J. Matter. Res. 8, 169 (1993).

    Google Scholar 

  2. A. Corma, A. Martínez, and C. Martínez, J. Catal. 149, 52 (1994).

    Google Scholar 

  3. T. López, J. Navarrete, R. Gómez, O. Novaro, F. Figueras, and H. Armendáriz, Appl. Catal. A 125, 217 (1995).

    Google Scholar 

  4. R.D. González, T. López, and R. Gómez, Catal. Today 35, 293 (1997).

    Google Scholar 

  5. G.M. Pajonk and A. El Tamany, React. Kinet. Catal. Lett. 2, 167 (1992).

    Google Scholar 

  6. C. Monterra, G. Cerrato, C. Emanuel, and V. Bolis, J. Catal. 142, 349 (1993).

    Google Scholar 

  7. B.E. Yoldas, J. Matter. Res. 5, 161 (1990).

    Google Scholar 

  8. J. Nair, P. Nair, J.G. van Ommen, J.R.H. Ross, and A.J. Burggraaf, J. Amer. Ceram. Soc. 81, 1487 (1998).

    Google Scholar 

  9. G.A. Danko, R. Silberglitt, P. Colombo, E. Pippel, and J. Woltersdorf, J. Amer. Ceram. Soc. 83, 1617 (2000).

    Google Scholar 

  10. J. Zhu, O. Palchik, S. Chen, and A. Gedanker, J. Phys. Chem. B 104, 7374 (2000).

    Google Scholar 

  11. G. Fetter, G. Heredia, L.A. Velázquez, A.M. Maubert, and P. Bosch, Appl. Catal. A 162, 41 (1997).

    Google Scholar 

  12. G. Fetter, F. Hernández, A.M. Maubert, V.H. Lara, and P. Bosch, J. Porous Mater. 4, 27 (1997).

    Google Scholar 

  13. B.L. Newalkar, J. Olanrewaju, and Komarneni, Chem. Mater. 13, 552 (2001).

    Google Scholar 

  14. S. Mintova, S. Mo, and T. Bein, Chem. Mater. 10, 4030 (1998).

    Google Scholar 

  15. I. Brawn, G. Schulz-Ekloff, D. Wöhrle, and W. Lautenschläger, Microporous Mesoporous Mater. 23, 79 (1998).

    Google Scholar 

  16. D.L. Boxall and C.M. Lukehart, Chem. Mater. 13, 806 (2001).

    Google Scholar 

  17. M. Magini and A. Cabrini, J. Appl. Crystallogr. 5, 14 (1972).

    Google Scholar 

  18. H.H. Kung, Stud. Surf. Sci. Catal., vol. 45 (1989), p. 124.

    Google Scholar 

  19. B.H. Davies, J. Amer. Ceram. Soc. 67, 168 (1984).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Fetter, G., Bosch, P. & López, T. ZrO2 and Cu/ZrO2 Sol-Gel Synthesis in Presence of Microwave Irradiation. Journal of Sol-Gel Science and Technology 23, 199–203 (2002). https://doi.org/10.1023/A:1013983211564

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/A:1013983211564

Navigation