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Structure, thermal behavior, and IR investigation of bis(3-amino-1,2,4-triazolium)monohydrogen monophosphate

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Abstract

Chemical preparation, calorimetric studies, crystal structure, and IR spectrometric investigation of (C2H5N4)2HPO4, denoted ATZP, are described. The compound crystallizes in the monoclinic system with C2/c space group. Its unit cell dimensions are a = 13.589(2) Å b = 11.105(2) Å c = 15.734(3) Å β = 104.68(2)°, V = 2296.8(7) Å3, and Z = 8. The structure of the title compound consists of a three dimensional network of H-bonds connecting all its components. The IR spectrum of ATZP is reported and discussed on the basis of group theoretical analysis.

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References

  1. Wolf, F.T. Nature Lond 1960, 188, 164.

    Google Scholar 

  2. Baouab, L.; Jouini, A. J. Solid State Chem. 1998, 141, 343.

    Google Scholar 

  3. Sheldrick, G.M. SHELX-97; University of Göttingen: Federal Republic of Germany, 1997.

    Google Scholar 

  4. Ferraris, G.; Ivaldi, G. Acta Crystallogr. B 1984, 40, 1.

    Google Scholar 

  5. Averbuch-Pouchot, M.T.; Durif, A.; Guitel, J.C. Acta Crystallogr. C 1988, 44, 1968.

    Google Scholar 

  6. Aoki, B.K.; Nagano, K.; Iitaka, Y. Acta Crystallogr. B 1971, 27, 11.

    Google Scholar 

  7. Baur, H.W. Acta Crystallogr. B 1974, 30, 1195.

    Google Scholar 

  8. Farrugia, L.J. J. Appl. Crystallogr. 1997, 30, 565.

    Google Scholar 

  9. Haile, S.M.; Kreuer, K.-D.; Maier, K. Acta Crystallogr. B 1995, 51, 680.

    Google Scholar 

  10. Brown, I.D. Acta Crystallogr. A 1976, 32, 24.

    Google Scholar 

  11. Lynch, D.E.; Dougall, T.; Smith, G.; Byriel, K.A.; Kennard, C.H.L. J. Chem. Crystallogr. 1999, 29, 67.

    Google Scholar 

  12. Nakamoto, K. Infrared and Raman Spectra of Inorganic and Coordination Compounds; Wiley: New York, 1986.

    Google Scholar 

  13. Steger, E.; Schmidt, W. Ber. Bruns. Phys. Chem. 1964, 68, 102.

    Google Scholar 

  14. Preston, C.M.; Adams, A.W. J. Phys. Chem. 1979, 83, 814.

    Google Scholar 

Download references

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Authors and Affiliations

  1. Laboratoire de Chimie du Solide, Département de Chimie, Faculté des Sciences de Monastir, Université du centre, 5019, Monastir, Tunisia, North Africa

    Leïla Baouab, Taha Guerfel, Monia Soussi & Amor Jouini

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  1. Leïla Baouab
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  2. Taha Guerfel
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  3. Monia Soussi
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  4. Amor Jouini
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Baouab, L., Guerfel, T., Soussi, M. et al. Structure, thermal behavior, and IR investigation of bis(3-amino-1,2,4-triazolium)monohydrogen monophosphate. Journal of Chemical Crystallography 30, 805–809 (2000). https://doi.org/10.1023/A:1013280426251

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  • DOI: https://doi.org/10.1023/A:1013280426251

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