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Reactions of 9,10-phenanthrenequinone and its nitro derivatives with acetone in the presence of Al2O3

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Abstract

The addition of acetone to 9,10-phenanthrenequinone and 2-nitro-, 2,7-dinitro-, and 2,4,7-trinitro-9,10-phenanthrenequinones in the presence of Al2O3 affords mono- and bisadducts. The crystal structures of 10-hydroxy-10-(2-oxopropyl)-2-nitro-9,10-dihydrophenanthren-9-one and 9,10″:10,9″-bishemiketal of 9,10-dihydroxy-2-nitro-9,10-bis(2-oxopropyl)-9,10-dihydrophenanthrene were determined.

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Authors and Affiliations

  1. Russian University of People"s Friendship, 6 ul. Miklukho-Maklaya, 117198, Moscow, Russian Federation

    R. V. Linko, A. V. Varlamov, B. E. Zaitsev & A. I. Chernyshev

  2. State Research Center of the Russian Federation “L. Ya. Karpov Research Physicochemical Institute,”, 10 ul. Vorontsovo Pole, 103064, Moscow, Russian Federation

    V. K. Belsky

Authors
  1. R. V. Linko
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  2. V. K. Belsky
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  3. A. V. Varlamov
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  4. B. E. Zaitsev
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  5. A. I. Chernyshev
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Linko, R.V., Belsky, V.K., Varlamov, A.V. et al. Reactions of 9,10-phenanthrenequinone and its nitro derivatives with acetone in the presence of Al2O3. Russian Chemical Bulletin 50, 1625–1629 (2001). https://doi.org/10.1023/A:1013042703773

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