Abstract
The reaction of 4,4-dimethyl-1,3-dioxane with bis(2-cyano)diethyl ether or 1,2-di(beta-cyanoethoxy)ethane yields the corresponding bis[2-(4,4-dimethyl-5,6-dihydro-2-oxazinyl)]diethyl ether and 1,2-di{beta-[2-(4,4-dimethyl-5,6-dihydro-2-oxazinyl)]ethoxy}ethane which are readily hydrolyzed under the action of aqueous alkali to give 3-methyl-3-amino-1-butanol.
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Kuznetsov, V.V., Mazepa, A.V., Brusilovskii, Y.E. et al. Reaction of 4,4-Dimethyl-1,3-dioxane with Dinitriles. Russian Journal of General Chemistry 71, 126–127 (2001). https://doi.org/10.1023/A:1012302127645
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DOI: https://doi.org/10.1023/A:1012302127645