Skip to main content
SpringerLink
Log in

Comparison of Capillary and Skimmer Interfaces in Evolved Gas Analysis-Mass Spectrometry (EGA-MS) with Regard to Impurities in Ceramic Raw Materials

  • Published:
Journal of Thermal Analysis and Calorimetry Aims and scope Submit manuscript

Abstract

Capillary and skimmer interfaces in EGA-MS were compared by analysis of the carbon substances remaining in the hydrolysis products of aluminum alkoxides. Peaks with higher intensities were detected in the skimmer interface mode than those in the capillary interface mode. It was confirmed in particular that the skimmer interface is effective in increasing the sensitivity for species with higher mass, e.g. the evolved butyl group, as carbon substances remaining in the hydrolysis product of aluminum sec-butoxide.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. T. Tsugoshi, M. Furukawa, M. Ohashi and Y. Iida, Anal. Sci., 15 (1999) 327.

    Article  CAS  Google Scholar 

  2. R. I. Zakharchenya and T. N. Vaislevskaya, J. Mater. Sci., 29 (1994) 2806.

    Article  CAS  Google Scholar 

  3. D. Papee, R. Fertian and R. Biais, Bull., Soc. Chem. France, (1958) 1301.

  4. D. C. Bradley, R. C. Mehrotra and D. P. Gaur, ‘Metal alkoxides’, Academic Press, London 1978.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Material Characterization Laboratory, Ceramic Science Department, National Industrial Research Institute of Nagoya, 462-8510, Nagoya, Japan

    T. Tsugoshi, M. Furukawa, M. Ohashi & Y. Iida

Authors
  1. T. Tsugoshi
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. M. Furukawa
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. M. Ohashi
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Y. Iida
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

About this article

Cite this article

Tsugoshi, T., Furukawa, M., Ohashi, M. et al. Comparison of Capillary and Skimmer Interfaces in Evolved Gas Analysis-Mass Spectrometry (EGA-MS) with Regard to Impurities in Ceramic Raw Materials. Journal of Thermal Analysis and Calorimetry 64, 1127–1132 (2001). https://doi.org/10.1023/A:1011528625590

Download citation

  • Issue Date:

  • DOI: https://doi.org/10.1023/A:1011528625590

Search

Navigation