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Mechanochemical Synthesis of Tri-μ2-Disulfido-μ3-Thio-Tris(Diethyldithiocarbamato)-S,S"-triangular- Trimolybdenum Diethyldithiocarbamate {Mo3(μ3-S)(μ2-S2)3[(C2H5)2NCS2]3}+[(C2H5)2NCS2]–

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Abstract

The mechanoactivated solid-state reaction of [Et4N]2[Mo3S7Br6] with Na(Et2NCS2) in a vacuum vibration ball mill yields the [Mo3S7(Et2NCS2)3]+[Et2NCS2]–complex. The product was studied by IR and Raman spectroscopy and differential thermal analysis.

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Authors and Affiliations

  1. Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent'eva 3, Novosibirsk, 630090, Russia

    V. V. Volkov, K. G. Myakishev & E. A. Il'inchik

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  1. V. V. Volkov
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  2. K. G. Myakishev
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  3. E. A. Il'inchik
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Volkov, V.V., Myakishev, K.G. & Il'inchik, E.A. Mechanochemical Synthesis of Tri-μ2-Disulfido-μ3-Thio-Tris(Diethyldithiocarbamato)-S,S"-triangular- Trimolybdenum Diethyldithiocarbamate {Mo3(μ3-S)(μ2-S2)3[(C2H5)2NCS2]3}+[(C2H5)2NCS2]–. Russian Journal of Coordination Chemistry 27, 398–400 (2001). https://doi.org/10.1023/A:1011387708782

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