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Synthesis and structure of a bis(ethynyl)-substituted oxahexacyclic cage ether

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Abstract

Intramolecular dehydration of a cage-diol results in the title compound. This crystallizes in the monoclinic space group P21/c; a = 8.6403(8), b = 9.5698(7), c = 14.062(1) Å β = 107.47(7)° and Z = 4.

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Authors and Affiliations

  1. Department of Chemistry, University of Houston, Houston, Texas, 77204

    Simon G. Bott

  2. Department of Chemistry, University of North Texas, Denton, Texas, 76203

    Alan P. Marchand & Kaipenchery A. Kumar

Authors
  1. Simon G. Bott
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  2. Alan P. Marchand
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  3. Kaipenchery A. Kumar
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Bott, S.G., Marchand, A.P. & Kumar, K.A. Synthesis and structure of a bis(ethynyl)-substituted oxahexacyclic cage ether. Journal of Chemical Crystallography 29, 347–349 (1999). https://doi.org/10.1023/A:1009586204669

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